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Students will learn about laboratory safety, basic laboratory equipment and experimental procedures used in inorganic and organic chemistry. Preparations and qualitative reactions will complement the theoretical knowledge of properties of elements and inorganic compounds. Working on several simple organic syntheses, students will acquire the requisite skills for the preparation and characterization of organic compounds. Final grade is based not only on the performance in the laboratory, but also on the knowledge of simple calculations (stoichiometry and preparation of solutions) and the chemical principles of procedures carried out.
Last update: Kubová Petra (02.01.2018)
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Students will be able to: work safely in a laboratory carry out basic laboratory operations combine the theoretical knowledge with experimental results understand the principles of organic synthesis - planning, building a reaction apparatus, carrying out a reaction, isolation and characterization of products write laboratory protocols Last update: Kubová Petra (02.01.2018)
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The subject is finished by completion of all laboratory works and continuous tests, submission of protocols and fulfillment of the finish test.
Last update: Mastný Libor (21.02.2018)
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R:Laboratory manual (for download from https://e-learning.vscht.cz/pluginfile.php/23433/mod_resource/content/3/Laborato%C5%99e%20oboru%20Bioinformatika%20I.pdf)
R:V. Jakeš & al.: Laboratoř anorganické chemie I, VŠCHT Praha, 2015, ISBN: 978-80-7080-941-9 (for download from https://e-learning.vscht.cz/pluginfile.php/15826/mod_resource/content/14/Jake%C5%A1%20LACH%20I%20.pdf)
A:D. Sýkorová, L. Mastný: Návody pro laboratoře z anorganické chemie, VŠCHT Praha, 2001, reprint 2009, ISBN: 80-7080-452-1
R:V. Flemr, E. Holečková: Úlohy z názvosloví a chemických výpočtů v anorganické chemii, VŠCHT Praha, 2001, ISBN: 80-7080-435-1
R: Šilhánková a kol.: Laboratoř organické chemie, VŠCHT Praha, 2000, dotisk 2007, 8070803959
R:Laboratory manual (for download from https://e-learning.vscht.cz/course/view.php?id=227) Last update: Kubová Petra (27.03.2019)
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1. Laboratory safety, rules, and protocols. 2. Basic inorganic laboratory equipment. 3. Basic laboratory procedures - dissolution, filtration, evaporation, precipitation, and decantation. 4. Basic laboratory operations - crystallization, weighing, determination of density, pH measurement. 5. Redox reactions - carrying out in solution and solid phase. 6. Chemistry of nonmetals - reactions of nonmetals and their compounds. 7. Important qualitative reactions of selected anions, their determination in an unknown sample. 8. Basic organic laboratory equipment. 9. Building of reaction apparatuses and basic operations in organic synthesis. 10. Selected one-step organic syntheses including isolation and identification of products, heating with stirring under a reflux condenser. 11. Crystallization in organic laboratory. 12. Extraction. 13. Distillation under ambient pressure. 14. Determination of melting point, GLC chromatography of compounds prepared. Last update: Kubová Petra (02.01.2018)
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Laboratory instructions, preparatory processes - video : https://e-learning.vscht.cz/course/view.php?id=227
Laboratory records: https://e-learning.vscht.cz/mod/url/view.php?id=3906
CLP pictograms for compounds and mixtures: https://prezi.com/embed/9pbb6hy3_was/?bgcolor=ffffff&lock_to_path=1&autoplay=no&autohide_ctrls=0
Safety in laboratory - video: https://e-learning.vscht.cz/mod/folder/view.php?id=3002
Basic laboratory procedures - video: https://e-learning.vscht.cz/mod/folder/view.php?id=3001 Last update: Mastný Libor (19.02.2018)
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Organic Chemistry I Last update: Kubová Petra (02.01.2018)
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| Teaching methods | ||||
| Activity | Credits | Hours | ||
| Účast v laboratořích (na exkurzi nebo praxi) | 1.5 | 42 | ||
| Příprava na přednášky, semináře, laboratoře, exkurzi nebo praxi | 0.5 | 14 | ||
| 2 / 2 | 56 / 56 | |||