SubjectsSubjects(version: 963)
Course, academic year 2021/2022
  
Water Analysis - Laboratory - M217012
Title: Laboratoř analytiky vody
Guaranteed by: Department of Water Technology and Environmental Engineering (217)
Faculty: Faculty of Environmental Technology
Actual: from 2019 to 2021
Semester: winter
Points: winter s.:5
E-Credits: winter s.:5
Examination process: winter s.:
Hours per week, examination: winter s.:0/8, MC [HT]
Capacity: unknown / 16 (10)
Min. number of students: unlimited
State of the course: taught
Language: Czech
Teaching methods: full-time
Teaching methods: full-time
Level:  
Note: course can be enrolled in outside the study plan
enabled for web enrollment
Guarantor: Kujalová Hana Ing. Ph.D.
Sýkora Vladimír doc. Ing. CSc.
Smrčková Štěpánka RNDr. Ph.D.
Class: Základní laboratoře
Classification: Chemistry > Analytical Chemistry
Interchangeability : N217020
Is interchangeable with: AM217012
Examination dates   Schedule   
This subject contains the following additional online materials
Annotation -
Students will learn to quantify the main components of drinking, surface and sewage. The acquired theoretical knowledge will be used in experimental activities and will acquire the necessary manual skills. Attention is focused not only on mastering the process but also on understanding the methodology, the proper processing of data and the interpretation of the results obtained. Methods of determination of individual analytes are applied to both model and real samples and during the semester, a basic analysis of drinking water is included in the program. The theoretical basics needed to master the Water Analysis Laboratory are lectured in the subject of Water Analysis.
Last update: Kujalová Hana (22.01.2018)
Aim of the course -

Students will be able to quantify basic components of drinking water, surface water and wastewater, and correctly interpret the results.

Last update: Kujalová Hana (22.01.2018)
Course completion requirements - Czech

Podmínkou pro získání zápočtu je absolvování všech úloh; při omluvené absenci lze omezený počet úloh absolvovat v náhradním termínu. Povinným výstupem z každé úlohy je zpracování naměřených dat ve formě protokolu. Výsledná známka vychází z průměrné známky za jednotlivá laboratorní cvičení.

Last update: Kujalová Hana (29.08.2023)
Literature -

Horáková M. a kol.: Analytika vody. Skriptum VŠCHT, Praha 2003, ISBN 978-80-7080-520-6

Pitter P.: Hydrochemie. Vydavatelství VŠCHT Praha 2015, ISBN 978-80-7080-928-0

Last update: Sýkora Vladimír (23.08.2024)
Requirements to the exam - Czech

Student je při každém laboratorním cvičení hodnocen z hlediska teoretických znalostí potřebných pro zvládnutí dané úlohy, dále z hlediska provedení experimentální části práce a zpracování získaných dat formou protokolu.

Last update: Kujalová Hana (29.08.2023)
Syllabus -

1. Safety and protection of health at work. The organizational instructions.

2. Taking laboratory places with equipment. Preparation of reagent solutions.

3. Preparation of calibration. Calibration for spectrophotometric determinations.

4. Spectrophotometric determination of ammonia, nitrite, nitrate, phosphorus, boron and silica.

5. Measurement of conductivity and pH value. Titration determination of alkalinity and acidity (calculation of carbon dioxide species), calcium and magnesium, chloride.

6. Determination of ion dissolved matter, dissolved matter and suspended solids. Titration determination of sulphate.

7. Spectrophotometric determination of ammonia, nitrite, nitrate, phosphorus and silica.

8. Determination of COD-Mn. Spectrophotometric determination of iron. Manganese determination by titration colorimetry.

9. Basic analysis of inorganic solids in drinking water.

9. Titration determination of dissolved oxygen. Titration and spectrophotometric determination of chlorine.

10. Determination of COD, BOD 7 (start) and TOC in wastewater. Determination of MBAS.

11. Completion of BOD 7. Detremination of hydrolyzable phosphate and total phosphorus.

12. Determination of inorganic, organic and Kjeldahl nitrogen in wastewater; the nitrogen balance.

13. Data processing and interpretation of the results.

14. Laboratory cleaning. Taking back of laboratory places with equipment.

Last update: Kujalová Hana (28.12.2022)
Learning resources -

http://tvp.vscht.cz/home/18861/18884

Last update: Kujalová Hana (29.08.2023)
Registration requirements - Czech

Laboratoř analytiky vody navazuje na předmět Analytika vody a využívá teoretických znalostí v něm získaných, proto je nutné souběžně absolvovat Analytiku vody (jedná se o korekvizitu).

Last update: Kujalová Hana (29.08.2023)
Teaching methods
Activity Credits Hours
Účast v laboratořích (na exkurzi nebo praxi) 4 112
Příprava na přednášky, semináře, laboratoře, exkurzi nebo praxi 1 28
5 / 5 140 / 140
 
VŠCHT Praha