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Instrumental methods used in analysis of organic and inorganic compounds in water including sample preparation are discussed: separation methods (chromatography - GC, GC-MS, HPLC, capillary isotachophoresis, ionic chromatography), spectral methods (AAS, ICP), total organic carbon (TOC), adsorbable and extractable organically bound halogens (AOX, EOX) and hydrocarbon index. Applicability of the methods is demonstrated during excursions.
Last update: Kubová Petra (12.04.2018)
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Students will be able to: use instrumental analytical methods for water analysis. Last update: Kubová Petra (12.04.2018)
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For the successful passing of the subject students are required to gain at least 51 point from overal number of 100 points in the written test. Last update: Kubová Petra (12.04.2018)
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R: M. Popl, J. Fähnrich: Analytická chemie životního prostředí (Environmental analytical chemistry), VŠCHT Praha 1999, ISBN 80-7080-336-3 A: J. Pawlyszin: Solid phase microextraction; theory and practice, Wiley-VCH, New York 1997, ISBN 0-471-19034-9 Last update: Kubová Petra (12.04.2018)
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Zkouška se koná jen písemnou formou na konci semestru. Opravnou zkoušku je možné konat během zkouškového období. Last update: Kubová Petra (12.04.2018)
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1. Introduction, guidelines, standards and required detection limits 2. Organic compounds, chromatographic methods (GC and HPLC), detection systems 3. Preconcentration and enrichment techniques for organic compounds 4. Derivatization, analyses of pesticides, PAHs, PCBs, volatile chlorinated hydrocarbons, haloforms, hydrocarbons 5. Capillary isotachophoresis 6. Heavy metals, atomic absorption spectroscopy 7. Total organic carbon, dissolved organic carbon, biochemical oxygen demand 8. Adsorbable and extractable organic chlorine (halogens) 9. Ionic chromatography 10. Gene probes 11. Excursion, demonstration 12. Excursion, demonstration 13. Excursion, demonstration 14. Test Last update: Kubová Petra (12.04.2018)
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http://www.vscht.cz/homepage/tvp/index Last update: Kubová Petra (12.04.2018)
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Analytical chemistry I Last update: Kubová Petra (12.04.2018)
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Teaching methods | ||||
Activity | Credits | Hours | ||
Příprava na zkoušku a její absolvování | 3 | 84 | ||
3 / 3 | 84 / 84 |