SubjectsSubjects(version: 949)
Course, academic year 2019/2020
  
Specialized Laboratory - Basic and Special Inorganic Technologies - M105014
Title: Laboratoř specializace - základní a speciální anorganické technologie
Guaranteed by: Department of Inorganic Technology (105)
Faculty: Faculty of Chemical Technology
Actual: from 2019
Semester: winter
Points: winter s.:7
E-Credits: winter s.:7
Examination process: winter s.:
Hours per week, examination: winter s.:0/10, MC [HT]
Capacity: unknown / unlimited (unknown)
Min. number of students: unlimited
Language: Czech
Teaching methods: full-time
Teaching methods: full-time
Level:  
For type: Master's (post-Bachelor)
Note: course can be enrolled in outside the study plan
enabled for web enrollment
Guarantor: Sedlářová Ivona Ing. Ph.D.
Class: Základní laboratoře
Examination dates   Schedule   
This subject contains the following additional online materials
Annotation -
Last update: Sedlářová Ivona Ing. Ph.D. (15.02.2018)
The aim of the course is to introduce students to the systematic laboratory work. Students pass the characteristic work in various laboratories of the department and get to know with the basic experimental techniques of inorganic technology field. Students who have completed all basic works continue under the guidance of their supervisor on a given topic that results from the selected specialization.
Aim of the course -
Last update: Sedlářová Ivona Ing. Ph.D. (15.02.2018)

Students will be able to:

  • conduct a given experiment
  • evaluate acquired data
  • prepare more extensive laboratory report
Literature -
Last update: Sedlářová Ivona Ing. Ph.D. (15.02.2018)

R:Novák J. a kol., Fyzikální chemie, skripta VŠCHT Praha, 2008, 8070806753

R:Lowell S., Shields J.E., Powder surface area and porosity, Chapman and Hall, London, 0412252406

according to instructions of work supervisor

Learning resources -
Last update: Sedlářová Ivona Ing. Ph.D. (15.02.2018)

http://uat.vscht.cz/cz/ke-stazeni/

Requirements to the exam -
Last update: Pátková Vlasta (04.01.2018)

For successful course pass:

test from each part must be at least 50% (1 possible repetition for each test)

exam consists from written and oral part

Syllabus -
Last update: Sedlářová Ivona Ing. Ph.D. (15.02.2018)

Schedule of laboratory work is specified to every student individually in the beginning of the semester.

List of experimental works:

1. Mercury porosimetry

2. Decomposition of raw materials by mineral acids

3. Characterization of photocatalytic active layers

4. Texture characterization of solids - BET method

5. Selectivity of membrane for gas separation

6. Measurement of microporous membranes permeation

7. Determination of kinetic parameters by electrochemical impedance spectroscopy

8. Cyclic voltametry

9. Characterization of the specific materiál surface properties

10. Determination of mass transfer coeff using a RDE

Registration requirements -
Last update: Sedlářová Ivona Ing. Ph.D. (15.02.2018)

Laboratory of Inorganic Chemistry I, Laboratory of Physical Chemistry I

Course completion requirements - Czech
Last update: Sedlářová Ivona Ing. Ph.D. (15.02.2018)

Zpracování a obhajoba protokolů z jednotlivých laboratorních prací.

Teaching methods
Activity Credits Hours
Účast v laboratořích (na exkurzi nebo praxi) 5 140
Obhajoba individuálního projektu 0.4 10
Příprava na přednášky, semináře, laboratoře, exkurzi nebo praxi 0.4 12
Práce na individuálním projektu 1.2 34
7 / 7 196 / 196
Coursework assessment
Form Significance
Regular attendance 10
Homework preparation 10
Report from individual projects 80

 
VŠCHT Praha