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Last update: Fialová Jana (20.12.2017)
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Last update: Fialová Jana (20.12.2017)
Students will be able to: Isolate and purify small amounts of compounds from natural materials Work with labware designed for semi-micro preparative scale Design procedures and equipment suitable for work with small amounts of compounds Perform spectral and other characterization from small amounts of isolated compounds |
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Last update: Fialová Jana (20.12.2017)
R: Mayo D. W., Pike R. M., Butcher S. S.: Microscale Oganic Laboratory , John Wiley and Sons, Inc., 2nd ed., New York, 1989 |
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Last update: Fialová Jana (20.12.2017)
Raich I., Medonos M.: Instructions for Isolation and separation methods: Laboratory, ICT Prague, 2012 |
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Last update: Fialová Jana (20.12.2017)
1. Labor safety in laboratory, construction of apparatuses for basic operations 2. Isolation of caffeine from tea, extraction, sublimation, melting point 3. Isolation of trehalose from yeast, deproteinization, HPLC verification of product purity 4. Isolation of piperine from black pepper, extraction, decantation, TLC, crystallization 5. Isolation of botulin from birch bark, extraction, crystallization, derivatization 6. Isolation of cinnamaldehyde from cinnamon using steam distillation 7. Isolation of D-glucosamine from crab shells, decalcification, hydrolysis, crystallization 8. GLC analysis of cinnamaldehyde 9. HPLC analysis of trehalose on ion-exchange resin 10. NMR spectra measurements of prepared samples 11. IR spectra measurements of prepared samples |
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Last update: Fialová Jana (20.12.2017)
Organic chemistry I Organic chemistry: Laboratory I |
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Last update: MORAVCOJ (27.02.2018)
Odevzdání preparátů a/nebo postupů vedoucímu práce. Zpracování experimentální činnosti do podoby písemného odborného sdělení a odevzdání vedoucímu práce.
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