SubjectsSubjects(version: 953)
Course, academic year 2015/2016
  
Analysis by Origin: Inorganic Materials - N402027
Title: Analýza z hlediska původu vzorku: anorganické materiály
Guaranteed by: Department of Analytical Chemistry (402)
Faculty: Faculty of Chemical Engineering
Actual: from 2010 to 2015
Semester: summer
Points: summer s.:4
E-Credits: summer s.:4
Examination process: summer s.:
Hours per week, examination: summer s.:1/2, C+Ex [HT]
Extent per academic year: 2 [hours]
Capacity: 10 / 10 (unknown)
Min. number of students: unlimited
State of the course: taught
Language: Czech
Teaching methods: full-time
Teaching methods: full-time
Level:  
Note: course can be enrolled in outside the study plan
enabled for web enrollment
Guarantor: Mestek Oto prof. Ing. CSc.
Examination dates   Schedule   
Annotation -
The course focuses mainly on chemical analysis (titration, gravimetric, photometric method) ores and other raw materials. The first part is devoted to decomposition of samples by acids and melting. The main part of the course is devoted to a review of methods of analysis of the most important metals (Fe, Mn, Al, As, Sb, Au, Ag, nonferrous metals, alkali metals and alkaline earth metals) and some non-metals (S, Si, P, P and C). The final part of the course is devoted to a review of chemical methods of water analysis (determination of major anions and cations, oxygen, chlorine, CO2, COD and BOD).
Last update: Mestek Oto (15.09.2013)
Aim of the course -

Students completing the course will gain theoretical and practical knowledge about the application of classical methods of chemical analysis (gravimetry and titration) on ore materials and surface and drinking water. They will learn various preparation methods: acid digestion and melting.

Last update: Mestek Oto (15.09.2013)
Literature -

R: Doležal J.: Povondra P., Šulcek Z.: Rozlady základních anorganických surovin, SNTL Praha 1966

A: Knipovič J.N., Moračevskij J.V.: Analiz miněralnovo syrja, GCHI Leningrad, 1956

R: Michal J. a kol.: Analýza rud a produktů jejich zpracování, SNTL Praha, 1984

R: Horáková M. a kol.: Chemické a fyzikální metody analýzy vod, SNTL Praha, 1986

Last update: VED402 (01.10.2013)
Learning resources -

http://www.vscht.cz/anl/paci/PAC/prezentace/Moderni%20analyticke%20metody%20v%20geologii.pdf

Last update: Mestek Oto (03.09.2013)
Requirements to the exam -

Passing labs and acknowledgement of protocols by assistant professor.

An oral examination supplemented by a simple calculation.

Student can use only two reparative terms.

Last update: Mestek Oto (15.09.2013)
Syllabus -

1. Sample decomposition by acid digestion

2. Sample decomposition by fusion

3. Analysis of iron ores

4. Analysis of ores of heavy metals

5. Analysis of ores of arsenic, antimony and tin

6. Analysis of ores of refractory metals

7. Analysis of ores of non-ferrous metals

8. Analysis of ores of gold and silver

9. Determination of alkali metal

10. Determination of alkali-earth metals

11. Determination of sulphur, phosphorous and boron

12. Determination of silica

13. Analysis of fresh and waste water I

14. Analysis of fresh and waste water II

Last update: Mestek Oto (18.05.2012)
Registration requirements -

Basic knowledge od analytical chemistry and minerology

Last update: Mestek Oto (03.09.2013)
Teaching methods
Activity Credits Hours
Konzultace s vyučujícími 0.5 14
Účast v laboratořích (na exkurzi nebo praxi) 1 28
Účast na přednáškách 0.5 14
Příprava na přednášky, semináře, laboratoře, exkurzi nebo praxi 1 28
Příprava na zkoušku a její absolvování 1 28
4 / 4 112 / 112
Coursework assessment
Form Significance
Report from individual projects 50
Examination test 25
Oral examination 25

 
VŠCHT Praha