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Poslední úprava: Staš Martin Ing. Ph.D. (16.09.2023)
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Poslední úprava: Staš Martin Ing. Ph.D. (16.09.2023)
M. Staš et al.: Analysis of Fuels - study text, 2023 (available via e-learning). M. Staš et al.: Hydrocarbon Analysis and Environment - powerpoint presentations (available via e-learning). S. Hála, M. Kuraš, M. Popl: Analysis of Complex Hydrocarbon Mixtures, Elsevier, 1981. ISBN: 0-444-99734-2. |
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Poslední úprava: Staš Martin Ing. Ph.D. (16.09.2023)
1. Introduction - classification of analytical methods, qualitative and quantitative analysis. 2. Separation methods in analysis (distillation, absorption, adsorption, extraction) - instrumentation, sample preparation and own execution, evaluation of results, examples. 3. Chromatography - introduction, classification, basic terminology, qualitative and quantitative analysis, areas of application. 4. Gas chromatography - columns, detectors, injectors, GC configuration, sample preparation for analysis, application examples. 5. Liquid chromatography (HPLC, LSC, GPC) - working conditions, instrumentation, detectors for LC, sample preparation, examples of use. 6. UV, fluorimetry - principle, advantages/disadvantages, instrumentation, sample preparation and own execution, quality/quantity, examples of use. 7. FTIR - principle, advantages/disadvantages, instrumentation, sample preparation and own execution, evaluation of results - quality/quantity, examples of use. 8. MS, NMR - principle, advantages/disadvantages, instrumentation, sample preparation and own execution, evaluation of results, examples of use. 9. Determination of metals and elements - AAS, AES, ICP, X-ray - principle, advantages/disadvantages, instrumentation, sample preparation and own execution, evaluation of results, examples of use. 10. Thermal methods - DTA, TGA, DSC, pyrolysis - principle, advantages/disadvantages, instrumentation, evaluation of results, examples of use. 11. Evaluation of the quality of gaseous fuels - an overview of monitored parameters, their importance, choice of appropriate methodologies for sampling and own analysis. 12. Evaluation of the quality of oil fractions and products - overview of monitored parameters, their significance, choice of appropriate analysis methodologies. 13. Evaluation of the quality of solid fuels and products of their processing - overview of monitored parameters, choice of appropriate methodologies for sampling and own analysis. 14. Special trace analyzes of selected pollutants - PAHs, PCBs, aldehydes, phenols, VOCs, sulfur substances, organometals; collection and preparation of samples. |
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Poslední úprava: Staš Martin Ing. Ph.D. (15.09.2023)
None. |
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Poslední úprava: Staš Martin Ing. Ph.D. (15.09.2023)
A successful completion of written and oral exam. |