Studenti budou umět:

Orientovat se v instrumentálních analytických metodách

Řešit konkrétní problémy analýzy reálných vzorků

Vyhodnocovat kvalitu a spolehlivost analytických výsledků

Intepretovat jednoduchá spektra získaná infračervenou spektroskopií, NMR spektroskopií a hmotnostní spektrometrií

The goal of Analytical chemistry II is to provide

• orientation in methods of instrumental analysis

• solve problems of real sample analysis

• evaluate quality and reliability of analytical results

• solve simple spectra measured by IR, H-NMR and MS

Z: Záruba a kol., Analytická chemie (1. díl ISBN 978-80-7080-950-1; 2. díl ISBN 978-80-7080-951-8), skripta VŠCHT Praha

D: Skoog, Holler, Nieman, Principles of Instrumental Analysis, Brooks/Cole Thomson Learning; 5. vydání (ISBN 9780030020780) a novější

D: Skoog, West, Holler, Crouch, Fundamentals of Analytical Chemistry, Brooks/Cole Thomson Learning; 5. vydání (ISBN 9780030020780) a novější

R: Skoog, Holler, Nieman, Principles of Instrumental Analysis, Brooks/Cole Thomson Learning; 5th edition (ISBN 9780030020780) and newer

A: Skoog, West, Holler, Crouch, Fundamentals of Analytical Chemistry, Brooks/Cole Thomson Learning; 5. vydání (ISBN 9780030020780) and newer

PDF soubory dostupné v rozhraní e-learning.vscht.cz

Další dkazy na elektronické zdroje budou poskytnuty na jednotlivých přednáškách.

PDF for the lectures available in e-learning.vscht.cz.

Other sources will be recommended during the lectures.

K předmětu jsou organizovány přednášky a cvičení pouze v ZS. V LS je možné skládat zkoušku, předmět však není přednášen (po dohodě jsou poskytovány konzultace) a rovněž nejsou organizována cvičení.

Every week of the winter semester there is a two hour lecture and one hour seminar. The lectures are concerned about principles, methods and theory. The seminars include practical calculations and solving of spectra. All seminars are held in computer laboratory.

1. Credit test is written during seminars in the 7th and 14th week. To get credits, a student has to obtain 50 % of the sum of the tests and 25 % of each test.

2. Students, who study in Czech, pass credit test in Czech. Students, who study in English, pass credit test in English.

3. It is necessary to have the Index (Student Book) with yourself during the writing of credit test. Exceptionally, the assistant can allow writing the test after checking the identity of the student using other ID with an up-to-date photograph.

4. Students register for a test using SIS (Educational Info System) and it is the duty of each student to sign in for the term listed there. Signing off is possible up to date listed in SIS. Later, it is possible only by request to the secretary of the department and only because of serious reasons. The test is failed when a student is absent and not signed off.

5. The assistant can allow writing the test when students arrive late. The missed time is not compensated.

6. It is not allowed to leave the room during the test. It is not allowed to use forbidden materials and other tools including telecommunication electronics.

7. Results of the test will be available in place and at the time, which will be announced at the beginning of the test.

8. The credits are written into the Index by the the assistant teaching seminars at the appointed time, which will be announced. Exceptionally, it is possible to arrange other time.

9. You can check your test at the assistant teaching seminars in place and at the time, which he or she assigns.

10. The examination is written and takes 50 min. It consists of ten questions. Examiner is allowed to ask further questions.

11. If some of the topics will not be given because of a holiday or a rector’s day, this is not a reason for exclusion of these topics from the examination test.

12. Students, who study in Czech, pass the examination in Czech. Students, who study in English, pass the examination in English.

13. Student has duty to present the Index with written credits during the examination, otherwise, it is impossible to start/continue the exam.

14. The students sign in for the examination using SIS and it is the duty of a student to sign in for the term listed here. Signing off is possible up to date listed in SIS. Later it is possible only by request to the secretary of the department and only because of serious reasons. The examination is classified „F“ when the student is absent and not signed off.

15. The assistant can allow writing examination when students arrive late. The missed time is not compensated.

16. It is not allowed to leave the room during the examination. It is not allowed to use forbidden materials and tools including telecommunication electronics.

17. The place and the time will be announced during the examination. The examiner assigns where and when will be possible to see checked examination test. If the student is not present in this time he or she resigns for any complaint and agree with the final classification. When the student does not agree with the classification of any of parts of the test, the examiner will provide one, exceptionally, more additional questions which will be answered in written form. According to the result of these additional questions the examiner can change overall classification.

18. Students can use only two reparative terms.

1. Nejistoty a testování hypotéz v analytické chemii

2. Vibrační spektrometrie - reflexní a mikroskopická IR; NIR a Ramanova spektrometrie

3. NMR spektrometrie - relaxace, chemická výměna, zobrazování metodou NMR

4. Pokročilé techniky hmostnostní spektrometrie

5. Spřažené techniky 1 - GC-MS, LC-MS, CE-MS

6. Spražené techniky 2 - GC/LC-ICP-MS, speciační analýza, LC/GC-IR, LC-NMR

7. Povrchová analýza 1 - fotony, elektrony, ionty

8. Povrchová analýza 2 - rastrovací sondou (STM, AFM, SNOM)

9. Analýza chirálních látek - úvod do chirálních separací a chioptických metod

10. Kinetické metody analýzy

11. Radioanalytické metody

12. Biochemická analýza

13. Chemické senzory a biosenzory

14. Procesní analýza

1. Uncertainties and testing of hypotheses in analytical chemistry

2. Vibrational spectrometry - reflection IR, IR microscopy, NIR spectrometry, Raman spectrometry

3. NMR spectrometry - relaxation, chemical exchange, NMR imaging

4. Enhanced mass spectrometry

5. Hyphenated techniques 1 - GC-MS, LC-MS, CE-MS

6. Hyphenated techniques 2 - GC/LC-ICP-MS, speciation analysis; LC/GC-IR, LC-NMR

7. Surface analysis 1 - by photons, electrons, ions

8. Surface analysis 2 - by a probe (STM, AFM, SNOM)

9. Analysis of chiral compounds - Introduction to chiral separation and chiroptic methods

10. Kinetic methods of analysis

11. Radioanalytical methods

12. Biochemical analysis

13. Chemical sensors and biosensors

14. Process analysis

Studující, kteří podle studijního plánu musí absolvovat Analytickou chemii I (N402002 nebo N402002A), ji musí mít zapsánu jako studijní povinnost v indexu a musí úspěšně složit zkoušku dříve než zkoušku z Analytické chemie II (N402004 nebo N402004A).

Students who according to the study plan must complete the course of Analytical chemistry I (N402002 or N402002A) must register the subject of Analytical chemistry I as an educational duty in the index and they must pass the exam before the exam in Analytical chemistry II (N402004 or N402004A).

Student by měl znát analytickou chemii v rozsahu vyučovaného předmětu Analytická chemie I (N402002). Dobrá znalost programu MS Excel 2007 (a novější) je nezbytná pro cvičení.

The students need to know analytical chemistry at the level of Analytical chemistry I (N402002). Sound knowledge of MS Excel 2007 (or later) is essential for seminars.