SubjectsSubjects(version: 855)
Course, academic year 2019/2020
  
Development and Optimisation of Procedures in Analytical Laboratory - D323020
Title: Vývoj a optimalizace postupů v analytické laboratoři
Guaranteed by: Department of Food Analysis and Nutrition (323)
Actual: from 2014
Semester: both
Points: 0
E-Credits: 0
Examination process:
Hours per week, examination: 0/0 other [hours/week]
Capacity: winter:unknown / unknown (unknown)
summer:unknown / unknown (unknown)
Min. number of students: unlimited
Language: Czech
Teaching methods: full-time
Level:  
For type:  
Note: course is intended for doctoral students only
can be fulfilled in the future
you can enroll for the course in winter and in summer semester
Guarantor: Poustka Jan prof. Dr. Ing.
Pulkrabová Jana doc. Ing. Ph.D.
Is interchangeable with: AP323003, P323003
This subject contains the following additional online materials
Annotation -
Last update: Poustka Jan prof. Dr. Ing. (03.03.2014)
The course is divided into two parts: 1. The proposal of the project in the field of laboratory work - the specification and evaluation of parameters of analytical procedures, economical balance; 2. The elaboration of the project focused on the overall balance of the practical realization of specific analytical procedures - students are provided with the corresponding project templates.
Aim of the course -
Last update: Poustka Jan prof. Dr. Ing. (03.03.2014)

Students will be able to:

1. Systematically process and evaluate the parameters of the analytical procedure

2. Systematically process and evaluate the economic indicators of the analytical procedure

3. Evaluate the feasibility and economy of the analytical procedure with regard to the practical requirements

4. Implement innovations in analytical procedures focused on reliability, speed and economy

Literature -
Last update: Poustka Jan prof. Dr. Ing. (03.03.2014)

The scientific publications and technical specifications including economic indicators - individually according to the topic of a given project

Learning resources -
Last update: Poustka Jan prof. Dr. Ing. (28.02.2014)

Students are provided with the corresponding project templates.

Syllabus -
Last update: Poustka Jan prof. Dr. Ing. (03.03.2014)

1. General strategies of the development and optimization of analytical procedures

2. Materials necessary for the analytical method optimization

3. Ways of the analytical procedure optimization

4. Optimizations of the izolation phase of analytical procedure - solvent extraction

5. Optimizations of the izolation phase of analytical procedure - solvent free extraction

6. Optimizations of the clean-up phase of analytical procedure

7. Optimizations of the instrumental determination - gas chromatography I

8. Optimizations of the instrumental determination - gas chromatography II

9. Optimizations of the instrumental determination - liquid chromatography I

10. Optimizations of the instrumental determination - liquid chromatography II

11. The cost and operational demands of the analytical procedure

12. The project proposal

13. The interim project control

14. The prezentation of the elaborated project and discussion

Registration requirements -
Last update: Poustka Jan prof. Dr. Ing. (28.02.2014)

No requirements.

Course completion requirements -
Last update: Poustka Jan prof. Dr. Ing. (03.03.2014)

The submission of the prepared project and its defense.

Coursework assessment
Form Significance
Defense of an individual project 100

 
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