SubjectsSubjects(version: 954)
Course, academic year 2023/2024
  
Water Analysis - M217010
Title: Analytika vody
Guaranteed by: Department of Water Technology and Environmental Engineering (217)
Faculty: Faculty of Environmental Technology
Actual: from 2023
Semester: winter
Points: winter s.:4
E-Credits: winter s.:4
Examination process: winter s.:
Hours per week, examination: winter s.:2/1, C+Ex [HT]
Capacity: 30 / 30 (unknown)
Min. number of students: unlimited
State of the course: taught
Language: Czech
Teaching methods: full-time
Teaching methods: full-time
Level:  
Note: course can be enrolled in outside the study plan
enabled for web enrollment
Guarantor: Sýkora Vladimír doc. Ing. CSc.
Kujalová Hana Ing. Ph.D.
Smrčková Štěpánka RNDr. Ph.D.
Interchangeability : N217018
Is interchangeable with: AM217010
This subject contains the following additional online materials
Annotation -
The methods used for water and wastewater analysis in laboratory are discussed in this course. The choice of methods is based on routine analytical practice. Students become acquainted with steps af analytical procedures, possible interferences, methods of sample pre-treatment, calculations and interpretation of results. Emphasis is also placed on understanding and practicing basic calculations used in solution preparation, data evaluation and results processing.
Last update: Kujalová Hana (17.09.2023)
Aim of the course -

Students will know the determination methodology of common components of drinking, surface and sewage water and they will know the principles of all determinations. Students will know the procedure of each hydroanalytic determination and they will be able to calculate the results from the measured values, including the correct interpretation of the obtained results.

Last update: Kujalová Hana (17.09.2023)
Literature -

Standard Methods for the Examination of Water and Wastewater. APHA,AWWA,WEF Washington 2012, ISBN 978-08-7553-013-0

Leo M.L. Nollet , Leen S.P. De Gelder: Handbook of Water Analysis. CRC Press, Boca Raton 2013, ISBN 978-1439889640

Last update: Kujalová Hana (17.09.2023)
Learning resources -

https://e-learning.vscht.cz/

Last update: Kujalová Hana (17.09.2023)
Requirements to the exam -

Students' knowledge and skills are tested in the form of a final test, which includes both closed and open questions from the theory and hydroanalytical calculations. The required range of knowledge corresponds to the syllabus of the course.

Last update: Kujalová Hana (17.09.2023)
Syllabus -

1. Mathematical processing of measured data in titration and spectrophotometric methods (including calibration)

2. Physico-chemical parameters: conductivity, pH. Application of ion-exchange in water analysis

3. Total inorganic parameters: total mineralisation, dissolved and suspended solids, ionic dissolved solids

4. Titration determination of neutralization capacity, calcium and magnesium

5. Titration determination of sulphates, chlorides

6. Spectrophotometric determination of ammoniacal nitrogen, nitrite, nitrate, reactive phosphorus, boron and silicon

7. Determination of COD-Mn; spectrophotometric determination of iron; determination of manganese by titration colorimetry

8. Iodometric determination of dissolved oxygen; titrimetric and spectrophotometric determination of reactive chlorine

9. Determination of COD, BOD, TOC and MBAS in surface water or wastewater

10. Determination of organic and ammoniacal nitrogen in wastewater

11. Determination of hydrolysable polyphosphates and total phosphorus

12. water analysis - scope, method of expressing results, checking accuracy

13. Sample collection, storage and preservation

14. Basics of quality control - limit of determination, limit of detection, measurement uncertainty, method validation

Last update: Kujalová Hana (17.09.2023)
Course completion requirements -

The course ends with a classified credit. The classification is based on the evaluation of the final test, which takes 90 minutes to write and no aids such as scripts, notes, tablet, notebook, etc. are allowed; only writing materials and a calculator are allowed. A maximum of 100 points can be obtained in the test, 70 for correctly answered questions and 30 for correctly calculated examples. The grading is based on the usual grading scale: 91-100 points A, 81-90 points B, 71-80 points C, 61-70 points D, 51-60 points E, 50 points or less F. There is one regular test date and two make-up dates, which can also be used to correct the grade. If you wish to make up a grade, you must inform the instructor to enter the grade of F in SIS, as this is the only way the system will allow you to register for the make-up term.

Last update: Kujalová Hana (17.09.2023)
Teaching methods
Activity Credits Hours
Konzultace s vyučujícími 0.5 14
Účast na přednáškách 1 28
Příprava na přednášky, semináře, laboratoře, exkurzi nebo praxi 1 28
Příprava na zkoušku a její absolvování 1 28
Účast na seminářích 0.5 14
4 / 4 112 / 112
Coursework assessment
Form Significance
Continuous assessment of study performance and course -credit tests 100

 
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