SubjectsSubjects(version: 855)
Course, academic year 2019/2020
  
Isolation and Separation of Molecules - M342005
Title: Izolace a separace molekul
Guaranteed by: Department of Chemistry of Natural Compounds (342)
Actual: from 2019
Semester: winter
Points: winter s.:4
E-Credits: winter s.:4
Examination process: winter s.:
Hours per week, examination: winter s.:2/1 C+Ex [hours/week]
Capacity: 24 / unlimited (unknown)
Min. number of students: unlimited
Language: Czech
Teaching methods: full-time
Level:  
For type: Master's (post-Bachelor)
Note: course can be enrolled in outside the study plan
enabled for web enrollment
Guarantor: Prokudina Elena Ing. Ph.D.
Annotation -
Last update: Kubová Petra Ing. (19.12.2017)
The course covers selected technological procedures from the point of view of a selection from alternative methods and possibilities how to affect efficiency and capacity of these operations. It emphasizes user view of unit technological operations.
Aim of the course -
Last update: Kubová Petra Ing. (19.12.2017)

Students will be able to:

Design a suitable isolation method

Optimize efficiency and capacity of an isolation method

Select a suitable separation method

Have an overview of technological aspects of discussed isolation and separation methods

Literature -
Last update: Kubová Petra Ing. (19.12.2017)

R: Fogler H.S.: Elements of Reaction Engineering,Prentice,Hall,New Jersey,2000,0130473944

Learning resources -
Last update: Kubová Petra Ing. (19.12.2017)

Lecture notes

Syllabus -
Last update: Kubová Petra Ing. (19.12.2017)

1. Introduction, formulation of a problem, process characterization

2. Separation of solid particles: filtration, microfiltration, ultrafiltration, centrifugation

3. Methods of suspension adjustments, effect of electrolytes, temperature, ionic strength, sorbents

4. Extraction and adsorption, comparison of basic parameters (equilibrium, interruptibility, efficiency, capacity, selectivity

5. Batch extraction, continuous extraction, Craig extraction, effect of pH, ion pairs formation

6. Batch adsorption, continuous adsorption, adsorption on a solid bed (approximation)

7. Chromatography: sorbents, instrumentation, implementation, mobile phase selection

8. Chromatography: Gauss equation, Poisson distribution, yield, and fraction purity

9. Chromatography: up-scaling

10. Precipitation, electrophoresis

11. Electro dialysis, isoelectric focusation

12. Crystallization, drying

13. Economic aspects of alternative methods, solvent regeneration, operation safety

14. Methods of choice

Registration requirements -
Last update: Kubová Petra Ing. (19.12.2017)

Organic chemistry

Mathematics I

General and inorganic chemistry

Course completion requirements - Czech
Last update: MORAVCOJ (23.02.2018)

Absolvování zápočtového testu minimálně na 50 %.

Ústní zkouška.

Coursework assessment
Form Significance
Regular attendance 20
Continuous assessment of study performance and course -credit tests 30
Oral examination 50

 
VŠCHT Praha