SubjectsSubjects(version: 853)
Course, academic year 2019/2020
  
Techniques of Measurement and Interpretation of IR and Raman Spectra - M402011
Title: Techniky měření a interpretace IČ a Ramanových spekter
Guaranteed by: Department of Analytical Chemistry (402)
Actual: from 2019
Semester: winter
Points: winter s.:2
E-Credits: winter s.:2
Examination process: winter s.:
Hours per week, examination: winter s.:1/0 Ex [hours/week]
Capacity: unlimited / unknown (unknown)
Min. number of students: unlimited
Language: Czech
Teaching methods: full-time
Level:  
For type:  
Additional information: http://www.vscht.cz/anl/matejka/index.html#techniky
Note: course can be enrolled in outside the study plan
enabled for web enrollment
Guarantor: Setnička Vladimír doc. Ing. Ph.D.
Prokopec Vadym Ing. Ph.D.
Interchangeability : N402030
Annotation -
Last update: Pátková Vlasta (05.01.2018)
The course introduces principles, experimental techniques and data interpretation of vibrational spectroscopy. Modern experimental techniques, spectral interpretation including practical examples are emphasized.
Aim of the course -
Last update: Pátková Vlasta (05.01.2018)

Students will be able to:

Explain principles of vibrational spectroscopy, to describe instrumentation used for infrared and Raman spectroscopy and microspectroscopy and the use of both spectroscopic techniques for analyses of samples in different states (gaseous, liquid and solid) considering both quantitative and structural informations.

Interpret infrared and Raman spectra of common organic compounds.

Literature -
Last update: Pátková Vlasta (05.01.2018)

R:George Socrates: Infrared and Raman Characteristic Group Frequencies: Tables and Charts, 3rd Edition, Wiley 2004, ISBN: 978-0-470-09307-8

Learning resources -
Last update: Pátková Vlasta (05.01.2018)

Spectool for Windows 2.1, A Hypermedia Book for Structure Elucidation of Organic Compounds with Spectroscopic Methods, Chemical Concepts, Weinheim 1994.

web of the ATHENS course - Introduction to Vibrational Spectroscopy http://www.vscht.cz/anl/vibspec/

Syllabus -
Last update: Pátková Vlasta (05.01.2018)

1. Principles of infrared spectroscopy, instrumentation

2. Classical measurement techniques of infrared spectra

3. Quantitative analysis using infrared spectroscopy

4. Surface analysis and microanalysis

5. Instrumentation for reflection techniques and infrared microscopy

6. Chemometric analysis of spectra

7. Principles of Raman spectroscopy

8. Raman spectroscopy and microscopy in near-infrared region

9. Raman spectroscopy and microscopy in visible spectral region

10. Optimization of experimental conditions in Raman spectroscopy

11. Quantitative analysis by Raman spectroscopy

12. Interpretation of infrared spectra

13. Interpretation of Raman spectra

14. Correlation of infrared and Raman spectra

Registration requirements -
Last update: Pátková Vlasta (05.01.2018)

none

Teaching methods
Activity Credits Hours
Účast na přednáškách 0,5 14
Příprava na zkoušku a její absolvování 1,5 42
2 / 2 56 / 56
Coursework assessment
Form Significance
Regular attendance 20
Examination test 80

 
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