SubjectsSubjects(version: 853)
Course, academic year 2019/2020
  
Doplnit - M402019
Title: Semestrální práce - analytická chemie a jakostní inženýrství I
Guaranteed by: Department of Analytical Chemistry (402)
Actual: from 2019
Semester: winter
Points: winter s.:4
E-Credits: winter s.:4
Examination process: winter s.:
Hours per week, examination: winter s.:0/4 MC [hours/week]
Capacity: unknown / unlimited (unknown)
Min. number of students: unlimited
Language: Czech
Teaching methods: full-time
Level:  
For type:  
Note: course can be enrolled in outside the study plan
enabled for web enrollment
Guarantor: Dolenský Bohumil doc. Ing. Ph.D.
Prokopec Vadym Ing. Ph.D.
Interchangeability : N402046
Annotation -
Last update: Pátková Vlasta (05.01.2018)
The semestral work I of the specialization analytical chemistry is focused on the understanding and interpretation of a combination of mass, vibrational and 1D and 2D NMR-spectra. Students have to determine the molecular structure of several substances interpreting the spectral data. The results of the project are presented both in the written form and as an oral contribution at a specialized seminar.
Aim of the course -
Last update: Pátková Vlasta (05.01.2018)

Students will be able to:

Interpret vibrational, mass and NMR spectra of organic compounds and considering mutual relationships to describe molecular structure of substances.

Present the spectral interpretation results and to discuss plausible explanations of observed spectral features.

Literature -
Last update: Pátková Vlasta (05.01.2018)

R:Structure Determination of Organic Compounds - Tables of Spectral Data (3rd Edition), By: Pretsch, E., Bühlmann, P., Affolter, C.; 2000 Springer - Verlag, ISBN: 978-3-540-67815-1, Electronic ISBN: 978-1-60119-351-3

A:George Socrates: Infrared and Raman Characteristic Group Frequencies: Tables and Charts, 3rd Edition, Wiley 2004, ISBN: 978-0-470-09307-8

Learning resources -
Last update: Pátková Vlasta (05.01.2018)

Spectool for Windows 2.1, A Hypermedia Book for Structure Elucidation of Organic Compounds with Spectroscopic Methods, Chemical Concepts, Weinheim 1994.

Syllabus -
Last update: Pátková Vlasta (05.01.2018)

In the first stage the students are introduced to software tools and literature for interpretation of vibrational, NMR and mass spectra. Afterwards they obtain a combination of vibrational, mass and 1D and 2D NMR spectra of unkknown substances. They consult the interpretation of spectra with teachers individually. The results are summarized in the form of a written protocol and a computer presentation to be presented as an oral contribution on a seminar. The seminar is attended by all student and teachers to discuss thoroughly individual spectra and to stress out relationships among both individual spectroscopic techniques and sample structures.

Registration requirements -
Last update: Pátková Vlasta (05.01.2018)

none

Teaching methods
Activity Credits Hours
Konzultace s vyučujícími 1 28
Obhajoba individuálního projektu 0,5 14
Práce na individuálním projektu 1,5 42
Účast na seminářích 1 28
4 / 4 112 / 112
Coursework assessment
Form Significance
Regular attendance 10
Defense of an individual project 50
Report from individual projects 40

 
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