SubjectsSubjects(version: 853)
Course, academic year 2019/2020
  
Trace and ultra-trace analysis - M402027
Title: Metody stopové a ultrastopové analýzy
Guaranteed by: Department of Analytical Chemistry (402)
Actual: from 2019
Semester: summer
Points: summer s.:4
E-Credits: summer s.:4
Examination process: summer s.:
Hours per week, examination: summer s.:2/1 C+Ex [hours/week]
Capacity: unknown / unknown (unknown)
Min. number of students: unlimited
Language: Czech
Teaching methods: full-time
Level:  
For type:  
Note: course can be enrolled in outside the study plan
enabled for web enrollment
Guarantor: Sýkora David doc. Dr. RNDr.
Sinica Alla Mgr. Ph.D.
Interchangeability : N402086
Examination dates   Schedule   
Annotation - Czech
Last update: Pátková Vlasta (05.01.2018)
Předmět je zaměřen na pochopení principů moderních operačních postupů analýzy pří stanovení stopového a ultrastopového množství analytů v matrici. Základem je získání přehledu o technikách přípravy vzorku pro danou oblast, řešení problematiky homogenity vzorku a interferenčních jevů. Studenti se seznámí s instrumentálními metodami a klasickými testy pro stopovou analýzu, a také se statistickými metodami hodnocení vhodnými pro ultrastopovou analýzu.
Aim of the course -
Last update: Pátková Vlasta (05.01.2018)

Students will expand and obtain new interdisciplinary knowledge in analytical and bioanalytical chemistry allowing them better orientation in the world of modern chemistry and to find applications in routine bioanalytical laboratories and in various fields of scientific and research activity, too.

Literature -
Last update: Pátková Vlasta (05.01.2018)

R: Beds P., Trace Analysis: A structured approach to obtaining reliable results, Editor(s): Prichard E., Points J., Mackay G. M., 1996, ISBN: 978-1-84755-940-1

R: Dean J. R., Methods for environmental trace analysis, John Wiley & Sons, 2003, ISBN: 0-470-84422-1

A: Lobinski R., Marczenko Z., Spectrochemical Trace Analysis for Metals and Metalloids, Elsevier, 1996, ISBN: 978-0-444-82368-7

A: Howard A. G., Statham P. J., Inorganic Trace Analysis: Philosophy and Practice, John Wiley & Sons, 1997, ISBN: 978-0-471-97672-1

Learning resources -
Last update: Pátková Vlasta (05.01.2018)

Prichard E., MacKay G. M., Points J., Trace Analysis: A Structured Approach to Obtaining Reliable Results (http://books.google.cz/books?isbn=0854044175 )

Syllabus -
Last update: Pátková Vlasta (05.01.2018)

1. Trace analysis and its significance in modern world. The definition of terms for trace and ultra-trace analyses

2. Difficulties in achieving reliable results at work with small amount of sample; procedures for their solution

3. Determination of sensitivity and detection limits for used methods. Requirements for standards, certified reference materials, chemicals

4. Requirements for process and laboratory equipment in trace analysis. Ways how to reduce contamination of samples

5. Representative sampling and material homogeneity; contamination and loss of analyte during analytical procedure

6. Sample stability and requirements for sample storage

7. Sample preparation in trace and ultra-trace analysis of inorganic and organic analytes. Processes of increasing analyte concentration. Enrichment techniques

8. Derivatization procedures, radioactive and non-radioactive labelling, and selection of suitable technique for determination of micro- and ultramicro amounts of analytes

9. Determination of micro-and ultramicro-amount analytes in biological samples

10. Instrumental methods in trace and ultra-trace analysis

11. Conventional tests and modern methods in trace and ultra-trace analysis

12. Trace analysis of technical samples, waters, airs and gases, foods and agricultural samples. Clinical and forensic analysis

13. Local and surface analyses; trace analysis over large distances

14. Assessment of correctness of the outputs obtained by trace analysis; errors of determination

Registration requirements
Last update: Pátková Vlasta (05.01.2018)

Analytical Chemistry I, II

Teaching methods
Activity Credits Hours
Konzultace s vyučujícími 0,5 14
Účast na přednáškách 1,5 42
Příprava na zkoušku a její absolvování 2 56
4 / 4 112 / 112
Coursework assessment
Form Significance
Regular attendance 20
Examination test 80

 
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