SubjectsSubjects(version: 853)
Course, academic year 2019/2020
  
Laboratory of atomic spectrometry - M402037
Title: Laboratoř atomové spektrometrie
Guaranteed by: Department of Analytical Chemistry (402)
Actual: from 2019
Semester: winter
Points: winter s.:2
E-Credits: winter s.:2
Examination process: winter s.:
Hours per week, examination: winter s.:0/2 MC [hours/week]
Capacity: unknown / unlimited (unknown)
Min. number of students: unlimited
Language: Czech
Teaching methods: full-time
Level:  
For type: Master's (post-Bachelor)
Note: course can be enrolled in outside the study plan
enabled for web enrollment
Guarantor: Mestek Oto prof. Ing. CSc.
Co-requisite : M402001
Annotation -
Last update: Mestek Oto prof. Ing. CSc. (23.01.2018)
In the laboratory, students learn the practical application of some of these techniques (different types of atomic absorption spectrometry, mass spectrometry, inductively coupled plasma and X-ray fluorescence spectrometry) for elemental analysis of major and trace amounts of elemets in various types of samples.
Aim of the course -
Last update: Mestek Oto prof. Ing. CSc. (23.01.2018)

Students completing the course will acquire practical knowledge of the methods of elemental analysis using optical spectrometry, X-ray spectrometry and mass spectrometry. They will be familiar with the various methods of sample preparation and problems of cleanness in trace laboratory.

Requirements to the exam -
Last update: Mestek Oto prof. Ing. CSc. (23.01.2018)

Passing labs and acknowledgement of protocols by assistant professor.

Syllabus -
Last update: Mestek Oto prof. Ing. CSc. (23.01.2018)

1. Atomic absorption spectrometry: determination of mercury using a single-purpose analyzer AMA.

2. Inductively coupled plasma mass spectrometry: determination of total element content.

3. Inductively coupled plasma spectrometry mass spectrometry: coupling with liquid chromatography for speciation analysis.

4. X-ray fluorescence spectrometry.

Registration requirements -
Last update: Mestek Oto prof. Ing. CSc. (23.01.2018)

Subject registration of the Laboratory of atomic spectrometry M402037 is conditioned by simultaneous registration of Atomic Spectrometry M402001.

Course completion requirements - Czech
Last update: Mestek Oto prof. Ing. CSc. (22.02.2018)

Studenti absolvují všechny laboratorní práce, vypracují a obhájí všechny protokoly.

Teaching methods
Activity Credits Hours
Konzultace s vyučujícími 0,2 6
Účast v laboratořích (na exkurzi nebo praxi) 1 28
Příprava na přednášky, semináře, laboratoře, exkurzi nebo praxi 0,8 22
2 / 2 56 / 56
Coursework assessment
Form Significance
Regular attendance 25
Homework preparation 25
Report from individual projects 50

 
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