SubjectsSubjects(version: 847)
Course, academic year 2018/2019
  
Analytical Chemistry I - N402002
Title in English: Analytická chemie I
Guaranteed by: Department of Analytical Chemistry (402)
Actual: from 2015 to 2018
Semester: summer
Points: summer s.:5
E-Credits: summer s.:5
Examination process: summer s.:
Hours per week, examination: summer s.:2/2 C+Ex [hours/week]
Capacity: 546 / 581 (unknown)
Min. number of students: unlimited
Language: Czech
Teaching methods: full-time
Level:  
For type:  
Additional information: http://předmět je vyučován pouze v letním semestru
http://www.vscht.cz/anl/bak01.html#druhy
http://www.vscht.cz/anl/cach1
Guarantor: Mestek Oto prof. Ing. CSc.
Záruba Kamil doc. Ing. Ph.D.
Interchangeability : N402002A, Z402002
Is interchangeable with: N402002A
In complex pre-requisite: N323003
This subject contains the following additional online materials
Annotation -
Last update: TAJ402 (23.01.2008)
Lectured methods include both classical chemical as well as instrumental techniques. The electrochemical analysis (potentiometry, voltammetry, polarography, coulometry), separation methods (gas and liquid chromatography) and atomic and molecular spectroscopy (atomic absorption and/or emission spectroscopy, infrared, visible and UV absorption, spectroscopy, nuclear magnetic resonance spectroscopy) are lectured. Separate lecture is devoted to mass spectrometry and another one to quality assurance procedures in analytical chemistry. The seminars are focused on gravimetric and titration calculations, calculation of equilibria, using of Nernst and/or Lambert-Beers Law and evaluation of basic characteristics of separation processes. The Analytical chemistry I is followed by Analytical chemistry II in next semester, which is application oriented.
Aim of the course -
Last update: VED402 (16.12.2013)

The aim of Analytical chemistry I is for student to learn analytical chemistry at basic level. Such student shall be able to specify his or her needs when communicating with analytical chemists or shall be able to perform analysis after enhancement of his/her knowledge of specific analytical technique.

Literature -
Last update: Záruba Kamil doc. Ing. Ph.D. (13.01.2017)

Skripta (czech): K. Záruba a kol., Analytická chemie, 1. a 2. díl, Vydavatelstvní VŠCHT Praha, 2016

R: D. Kealey, P. J. Haines: Analytical Chemistry, BIOS Sci. Publ., Oxford 2002, ISBN 1-85996-189-4

Learning resources -
Last update: VED402 (02.10.2013)

http://vydavatelstvi.vscht.cz/knihy/uid_es-004

http://vydavatelstvi.vscht.cz/katalog/uid_isbn-978-80-7080-743-9

Teaching methods -
Last update: TAJ402 (23.01.2008)

Every week there is a two hour lecture and one hour seminar. The lectures are concerned about principles, methods and theory. The seminars include practical calculations of titration and gravimetric stoichiometry and pH, complex stability and other equlibria important for analytical chemistry.

Requirements to the exam -
Last update: Záruba Kamil doc. Ing. Ph.D. (01.07.2019)

1. Two Continuous Credit tests (50 min.) are written during the semester, the first one in the 8th and the second one in the 13th week of the semester. The tests are written at other time and place than the seminar, it is necessary to apply for the term in Educational Info System (student.vscht.cz, SIS). Each test is graded out of 100 points, a maximum total score of the two tests being 200 points. In order to obtain the Credit, it is necessary to score at least 100 points in the total and also to score at least 25 points in each Continuous test.

It is possible to gain bonus points in the Continuous Credit tests that are added to the score of the regular Examination test (but not to the reparative Examination test):

(total score of the two Continous tests - 100) / 10 to be round up to integer number = number of bonus points

E.g. total score up to 104 points = no bonus point, total score 105-114 points = 1 bonus point, total score 195-200 points = 10 bonus points.

Fail or absence on the Continous Credit Test may be redeemed through the Comprehensive Credit test (100 min.) which combines the thematics of the two Continuous Credit tests. The maximum score of the Comprehensive Credit test is 200 points, it is necessary to score at least 100 points and also at least 25 points in each of the two parts (corresponding to Continuous Tests) to obtain the Credit. Three terms for the Comprehensive Credit test are offered during the last week of the semester and an examination period. Student can use only two of these terms.

2. Students, who study in Czech, pass credit test in Czech. Students, who study in English, pass credit test in English.

3. It is necessary to have Index (Study Record Book) with yourself during the writing of Comprehensive credit test. Exceptionally, the assistant can allow writing the test after checking the identity of a student using other IDs with up to date photograph.

4. The students sign in for Comprehensive credit test using SIS and it is duty of student to sign in for the term listed here. Signing off is possible up to date listed in SIS. Later it is possible only by request to the secretary of the department and only because of serious reasons. The test is failed when the student is absent and not signed off.

5. The assistant can allow writing test (both Comprehensive or Continous) when a student arrives late. The missed time is not compensated.

6. It is not allowed to leave the room during the test. It is not allowed to use forbidden materials and tools including telecommunication tools and calculators with the memory allowing store mathematical formulas.

7. The results of the Comprehensive test will be available on the place and in time, which will be announced at the beginning of the test.

8. The Credits are written into the Index by assistant teaching seminars in time, which will be announced. Exceptionally it is possible to agree other time.

9. You can check your test at assistant teaching seminars in time and on place, which he or she assigns.

10. The examination is written and takes 100 min.

11. Students, who study in Czech, pass an examination in Czech. Students, who study in English, pass an examination in English.

12. The student is obliged to present Index with written credit during the examination, otherwise, it is impossible to continue in examination.

13. The students register for the examination using SIS and it is the duty of a student to sign in for the term listed here. Signing off is possible up to date listed in SIS. Later it is possible only by request to the secretary of the department and only because of serious reasons. The examination is classified "F" when a student is absent and not signed off.

14. The assistant can allow writing examination when a student arrives late. The missed time is not compensated.

15. It is not allowed to leave the room during an examination. It is not allowed to use forbidden materials and tools including telecommunication tools and calculators.

16. The place and time will be announced during the examination. The examiner assigns where and when will be possible to see checked examination test. If the student is not present at this time he or she resigns for any complain and agree with results. When a student does not agree with the classification of any of parts of the test, the examiner will provide one, exceptionally more, additional questions which will be answered in written form. According to the result of these additional questions, the examiner is allowed to change the overall classification.

17. Student can use only two reparative terms.

Syllabus -
Last update: Mestek Oto prof. Ing. CSc. (09.01.2015)

1. Basic terms in analytical chemistry, equilibria in aqueous solutions

2. Equilibria in aqueous solutions, pH

3. Volumetric and gravimetric analysis

4. Electroanalytical methods

5. Electroanalytical methods

6. Principles of spectrometry, spectrometric instrumentation

7. Atomic spectrometry

8. Molecular spectrometry

9. Molecular spectrometry

10. Extraction, principles of chromatography

11. Principles of chromatography, gas chromatography

12. Liquid chromatography, electrophoresis

13. Mass spectrometry

14. Errors of analytical measurements

Entry requirements -
Last update: TAJ402 (23.01.2008)

The student needs to know both inorganic and organic chemistry nomenclature, physical principles (magnetism, electromagnetic radiation etc.) and mathematics (polynomials). Sound knowledge in computing with logarithms and percents is essential.

Registration requirements -
Last update: VED402 (12.09.2013)

No

Teaching methods
Activity Credits Hours
Konzultace s vyučujícími 0,5 14
Účast na přednáškách 1 28
Příprava na přednášky, semináře, laboratoře, exkurzi nebo praxi 1 28
Příprava na zkoušku a její absolvování 1,5 42
Účast na seminářích 1 28
5 / 5 140 / 140
Coursework assessment
Form Significance
Examination test 50
Continuous assessment of study performance and course -credit tests 50

 
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