SubjectsSubjects(version: 853)
Course, academic year 2019/2020
  
Doplnit ! - P402005
Title: Separační metody pro doktorandy
Guaranteed by: Department of Analytical Chemistry (402)
Actual: from 2019
Semester: summer
Points: summer s.:0
E-Credits: summer s.:0
Examination process: summer s.:
Hours per week, examination: summer s.:2/1 other [hours/week]
Capacity: unknown / unknown (unknown)
Min. number of students: unlimited
Language: Czech
Teaching methods: full-time
Level:  
For type: doctoral
Additional information: https://e-learning.vscht.cz/
Note: course is intended for doctoral students only
can be fulfilled in the future
Guarantor: Sýkora David doc. Dr. RNDr.
Řezanka Pavel doc. RNDr. Ing. Ph.D.
Interchangeability : D402010
Is interchangeable with: AP402005
Examination dates   Schedule   
Annotation -
Last update: Sýkora David doc. Dr. RNDr. (31.08.2018)
Students will gain practically utilizable information on modern separation techniques, specifically liquid, gas, and supercritical chromatography, capillary electrophoresis, and mass spectrometry. Principles of the methods will be summarized. Then modern instruments will be shown and troubleshooting discusses. The practical case studies will be analyzed in detail and a potential of modern instrumentation for solution of complex analytical tasks will be demonstrated. Each student will receive a specific topic to cover in its bibliographic search and he/she will prepare presentation for the peers.
Aim of the course -
Last update: Sýkora David doc. Dr. RNDr. (31.08.2018)

Students will gain:

new practically applicable skills in the area of up-to-date separation methods

knowledge how troubleshoot a modern instrumentation

insight to the analysis of complex samples utilizing advanced separation methods

practical experience with moder instrumentation

abilities related with elaboration of a bibliographical search and its prezentation

Literature -
Last update: Sýkora David doc. Dr. RNDr. (12.10.2018)

A:High Performance Capillary Electrophoresis - D.N. Heiger, Agilent, 2000.

A:Introduction to Modern Liquid Chromatography - book, L.R. Snyder, J.J. Kirkland and J.W. Dolan, Wiley, 2010, ISBN:978-0-470-16754-0.

A:Gas Chromatography and Mass Spectrometry-A Practical Guide - book, O.D. Sparkman, Z.E. Penton, and F.G. Kitson, 2011, Elsevier, ISBN:978-0-12-373628-4.

A:Introduction to Mass Spectrometry - book, J.T. Watson and O.D. Sparkman, Wiley, 2007, ISBN: 978-0-470-51634-8.

Teaching methods -
Last update: Sýkora David doc. Dr. RNDr. (31.08.2018)

Lectures, seminars, practical demonstrations, presentations.

Syllabus -
Last update: Sýkora David doc. Dr. RNDr. (28.08.2018)

1) Principles of gas (GC), liquid (LC) and supercritical fluid chromatography

2) Principles of capillary electrophoresis (CE) a mass spectrometry (MS)

3) Multidimensional techniques of GC

4) GC troubleshooting

5) Practical demonstration of instrumentation and selected case studies in GC

6) Multidimensional techniques of LC

7) LC troubleshooting

8) Practical demonstration of instrumentation and selected case studies in LC

9) Case studies in the forensic analysis

10) Case studies in the analysis of pharmaceuticals

11) Case studies in the analysis of drugs

12) Modern chiral separations in the field of CE

13) Practical demonstration of instrumentation and selected case studies in CE

14) Presentation of bibliography search projects

Entry requirements -
Last update: Sýkora David doc. Dr. RNDr. (31.08.2018)

Separation methods - graduate level.

Registration requirements -
Last update: Sýkora David doc. Dr. RNDr. (31.08.2018)

Analytical chemistry - bachelor's level.

Course completion requirements -
Last update: Sýkora David doc. Dr. RNDr. (01.09.2018)

The final assessment is based on the evaluation of written test exam and quality of individual bibliography search project including presentation.

Coursework assessment
Form Significance
Defense of an individual project 40
Examination test 60

 
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