SubjectsSubjects(version: 955)
Course, academic year 2023/2024
Separation methods for PhD students - P402005
Title: Separační metody pro doktorandy
Guaranteed by: Department of Analytical Chemistry (402)
Faculty: Faculty of Chemical Engineering
Actual: from 2023 to 2023
Semester: summer
Points: summer s.:0
E-Credits: summer s.:0
Examination process: summer s.:
Hours per week, examination: summer s.:2/1, other [HT]
Capacity: unknown / unknown (unknown)
Min. number of students: unlimited
State of the course: taught
Language: Czech
Teaching methods: full-time
Teaching methods: full-time
Additional information:
Note: course is intended for doctoral students only
can be fulfilled in the future
Guarantor: Sýkora David prof. Dr. RNDr.
Řezanka Pavel doc. RNDr. Ing. Ph.D.
Is interchangeable with: AP402005
This subject contains the following additional online materials
Annotation -
Students will gain new information on modern separation techniques, specifically liquid, gas, and supercritical chromatography, capillary electrophoresis, and mass spectrometry. Principles of the methods will be summarized. Potential of modern instrumentation for solution of complex analytical tasks will be demonstrated with the emphasis on multidimensional separations. Each student will receive a specific topic to cover in its bibliographic search and he/she will prepare presentation for the peers.
Last update: Sýkora David (03.05.2022)
Aim of the course -

Students will gain:

new knowledge in the area of up-to-date separation methods

insight to the analysis of complex samples utilizing advanced separation methods

abilities related with elaboration of a bibliographical search and its prezentation

Last update: Sýkora David (03.05.2022)
Literature -

A:Two-Dimensional Liquid Chromatography - firemní příručka. P.W. Carr, D.R. Stoll, Agilent, 2016.

A:High Performance Capillary Electrophoresis - D.N. Heiger, Agilent, 2000.

A:Introduction to Modern Liquid Chromatography - book, L.R. Snyder, J.J. Kirkland and J.W. Dolan, Wiley, 2010, ISBN:978-0-470-16754-0.

A:Gas Chromatography and Mass Spectrometry-A Practical Guide - book, O.D. Sparkman, Z.E. Penton, and F.G. Kitson, 2011, Elsevier, ISBN:978-0-12-373628-4.

A:Introduction to Mass Spectrometry - book, J.T. Watson and O.D. Sparkman, Wiley, 2007, ISBN: 978-0-470-51634-8.

Last update: Sýkora David (03.05.2022)
Teaching methods -

Lectures, seminars, practical demonstrations, presentations.

Last update: Sýkora David (31.08.2018)
Syllabus -

1) Principles of gas (GC), liquid (LC) and supercritical fluid chromatography

2) Principles of capillary electrophoresis (CE) a mass spectrometry (MS)

3) Multidimensional techniques of GC I

4) Multidimensional techniques of GC II

5) Multidimensional techniques of GC III

6) Multidimensional techniques of LC I

7) Multidimensional techniques of LC II

8) Multidimensional techniques of LC III

9) Case studies in the forensic analysis

10) Case studies in the analysis of pharmaceuticals

11) Modern chiral separations in the field of CE

12) Chiral selectors in CE

13) Presentation of bibliography search projects I

14) Presentation of bibliography search projects II

Last update: Sýkora David (03.05.2022)
Entry requirements -

Separation methods - graduate level.

Last update: Sýkora David (31.08.2018)
Registration requirements -

Analytical chemistry - bachelor's level.

Last update: Sýkora David (31.08.2018)
Course completion requirements -

The final assessment is based on the evaluation of written test exam and quality of individual bibliography search project including presentation.

Last update: Sýkora David (01.09.2018)