SubjectsSubjects(version: 954)
Course, academic year 2023/2024
  
Inorganic Chemistry: Laboratory I - B101004
Title: Laboratoř anorganické chemie I
Guaranteed by: Department of Inorganic Chemistry (101)
Faculty: Faculty of Chemical Technology
Actual: from 2022 to 2023
Semester: summer
Points: summer s.:3
E-Credits: summer s.:3
Examination process: summer s.:
Hours per week, examination: summer s.:0/4, MC [HT]
Capacity: unknown / unknown (unknown)
Min. number of students: unlimited
State of the course: taught
Language: Czech
Teaching methods: full-time
Teaching methods: full-time
Level:  
Old code: ACH1L
Note: deregister from the exam date if a requisite was not fulfilled
enabled for web enrollment
Guarantor: Mastný Libor Ing. CSc.
Jakeš Vít Ing. Ph.D.
Class: Základní laboratoře
Pre-requisite : {prerekvizita pro Laboratoř z anorganické chemie I ("výpočty")}, {x}
Interchangeability : AB101004, N101003, N101003A
Is incompatible with: V832005
Is pre-requisite for: B110012
Is interchangeable with: AB101004
In complex pre-requisite: AB110005, B110005
This subject contains the following additional online materials
Annotation -
Students are acquainted with the principles of work safety, basic laboratory equipment and basic experimental procedures. Preparation tasks and qualitative chemical reactions complement students' theoretical knowledge of the characteristic properties of the elements and compounds.
Last update: Jakeš Vít (29.01.2018)
Aim of the course -

Students will be able

  • to move safely in a laboratory;
  • to perform basic laboratory procedures;
  • to combine theoretical knowledge with experimental outputs;
  • to evaluate independently results of their work and make a detailed task description in the final record.
Last update: Jakeš Vít (29.01.2018)
Literature -

V. Jakeš a kol.: Laboratoř anorganické chemie I, VŠCHT Praha, 2018, ISBN: 978-80-7592-015-7 (available for download at: https://e-learning.vscht.cz/pluginfile.php/39052/mod_resource/content/3/LACH_I_skriptum_Jakeskol_2ed%282019%29.pdf)

D. Sýkorová, L. Mastný: Návody pro laboratoře z anorganické chemie, VŠCHT Praha, 2001, reprint 2009, ISBN: 80-7080-452-1

V. Flemr, E. Holečková: Úlohy z názvosloví a chemických výpočtů v anorganické chemii, VŠCHT Praha, 2001, ISBN: 80-7080-435-1

Last update: Jakeš Vít (01.08.2019)
Learning resources -

Programme of the Inorganic Chemistry: Laboratory I course and preparatory processes (video): https://e-learning.vscht.cz/course/view.php?id=40

Laboratory records: https://e-learning.vscht.cz/mod/url/view.php?id=3906

CLP pictograms for compounds and mixtures: https://prezi.com/embed/9pbb6hy3_was/?bgcolor=ffffff&lock_to_path=1&autoplay=no&autohide_ctrls=0

Safety in laboratory - video: https://e-learning.vscht.cz/mod/folder/view.php?id=3002

Basic laboratory procedures - video: https://e-learning.vscht.cz/mod/folder/view.php?id=3001

Last update: Jakeš Vít (29.01.2018)
Requirements to the exam -
  • regular tests in the beginning of each laboratory day (theoretical background and laboratory calculation)
  • final test (knowledge based on laboratory work and laboratory calculation)
  • reports from chosen laboratory tasks

Last update: Jakeš Vít (13.02.2018)
Syllabus -

1. Work safety in laboratory, laboratory rules, laboratory records.

2. Basic laboratory equipment.

3. Essential laboratory procedures - dissolution, filtration, evaporation, precipitation, decantation, work with a test tube.

4. Essential laboratory operations - crystallization, weighing, determination of density, pH determination.

5. Oxidation-reduction reactions - carried out in solution and in solid state.

6. Chemistry of non-metals - reactions of non-metals and their compounds.

7. Preparation of important compounds of selected elements and their reactions.

8. Important qualitative reactions of anions and their determination in unknown samples.

9. Chemistry of metals - reactions of metals and their compounds.

10. Coordination compounds of transition metals.

11. Qualitative reactions of cations, their separation and identification in unknown samples.

12. Mass balance of preparative experiments.

Last update: Jakeš Vít (29.01.2018)
Registration requirements -

General and Inorganic Chemistry I (AB101001)

Chemical and Balance Calculation (AB101003)

Last update: Jakeš Vít (01.08.2019)
Course completion requirements -

The subject is finished by completion of all laboratory works and continuous tests, submission of protocols and fulfillment of the finish test.

  • regular tests in the beginning of each laboratory day (theoretical background and laboratory calculation)
Last update: Mastný Libor (21.02.2018)
Teaching methods
Activity Credits Hours
Účast v laboratořích (na exkurzi nebo praxi) 2 56
Příprava na přednášky, semináře, laboratoře, exkurzi nebo praxi 1 28
3 / 3 84 / 84
 
VŠCHT Praha