Advanced Methods of Polymer Analysis - M112017
Title: Pokročilé metody analýzy polymerů
Guaranteed by: Department of Polymers (112)
Faculty: Faculty of Chemical Technology
Actual: from 2024
Semester: winter
Points: winter s.:3
E-Credits: winter s.:3
Examination process: winter s.:
Hours per week, examination: winter s.:2/0, Ex [HT]
Capacity: unlimited / unknown (unknown)
Min. number of students: unlimited
State of the course: taught
Language: Czech
Teaching methods: full-time
Teaching methods: full-time
Level:  
Note: course can be enrolled in outside the study plan
enabled for web enrollment
Guarantor: Merna Jan prof. Ing. Ph.D.
Hrdlička Zdeněk doc. Ing. Ph.D.
Classification: Chemistry > Analytical Chemistry
Interchangeability : N112045
Examination dates   
This subject contains the following additional online materials
Annotation -
The course focuses on advanced methods of analysis of polymeric materials, e.g. measurement of rheological, mechanical, thermal and spectroscopic properties. Emphasis is placed on the relationship between structure and properties of materials. The course extends and builds on the undergraduate course B112003 Characterization of Polymers and other courses focused on polymeric materials.
Last update: Hrdlička Zdeněk (13.09.2024)
Aim of the course -

Students will be able to:

orient themselves in the methods of analysis of polymeric substances

select the appropriate method for determining the essential properties of polymers

Last update: Hrdlička Zdeněk (13.09.2024)
Course completion requirements - Czech

Průběžný a zkouškový test.

Last update: Hrdlička Zdeněk (13.09.2024)
Literature - Czech

Povinná:

  • Podzimek, Štěpán. Light scattering, size exclusion chromatography and asymmetric flow field flow fractionation, powerful tools for the characterization of polymers, proteins and nanoparticles. Hoboken: Wiley, 2011, s. ISBN 978-0-470-38617-0.
  • Malkin A.Y., Isayev A.I.. Rheology. Concepts, Methods & Applications.. Toronto: ChemTec Publishing, 2006, s. ISBN 9781895198331.

Doporučená:

  • Striegel, André M.. Modern size-exclusion liquid chromatography, practice of gel permeation and gel filtration chromatography. Hoboken: Wiley, 2009, s. ISBN 978-0-471-20172-4.
  • Ward, I.M., Hadley, D.W.. An Introduction to the Mechanical Properties of Solid Polymers. Chichester: Xiley, 1998, s. ISBN 0-471-93887-4.
  • Mills, N. J.. Plastics, microstructure and [engineering] applications. Amsterdam: Elsevier, 2005, https://vufind.techlib.cz/Record/000171972 s. ISBN 0-7506-5148-2.
  • Strobl, Gert R.. The physics of polymers, concepts for understanding their structures and behavior. Berlin ;, New York: Springer, 2007, https://vufind.techlib.cz/Record/000940269 s. ISBN 978-3-540-25278-8.

Last update: Hrdlička Zdeněk (13.09.2024)
Requirements to the exam - Czech

Průběžný a zkouškový test.

Last update: Hrdlička Zdeněk (13.09.2024)
Syllabus -

1. Introduction, structure vs. properties of polymers

2. Composition of polymeric materials (polymers and additives)

3. Degradation and stabilization of polymeric materials

4. Methods for characterizing thermal properties (DSC, DMA, TGA)

5. Spectroscopic methods (UV, IR, NMR)

6. Methods for determining the molar mass of polymers

7. Fractionation of polymers

8. Flow properties of polymers, viscosity, influence of external factors on viscosity

9. Measurement of viscosity of polymeric substances: rotational and capillary viscometers

10. Viscosity measurements of polymeric substances: plate plastometers, ball and special viscometers

11. Determination of crosslinking characteristics of rubber compounds and thermosets

12. (Quasi)-static mechanical testing of polymeric materials

13. Dynamic mechanical testing of polymeric materials

14. Methods of surface analysis of polymeric materials (optical microscopy, SEM, TEM, AFM)

Last update: Hrdlička Zdeněk (13.09.2024)
Learning resources -

selected presentations available from teacher or in the e-learning

Last update: Hrdlička Zdeněk (13.09.2024)
Entry requirements - Czech

Jsou vyžadovány základní znalosti makromolekulární chemie.

Last update: Hrdlička Zdeněk (13.09.2024)
Registration requirements -

Macromolecular chemistry

Last update: Hrdlička Zdeněk (13.09.2024)