SubjectsSubjects(version: 954)
Course, academic year 2023/2024
  
Chromatography and mass spectrometry: Laboratory - M323022
Title: Laboratoř chromatografie a hmotnostní spektrometrie
Guaranteed by: Department of Food Analysis and Nutrition (323)
Faculty: Faculty of Food and Biochemical Technology
Actual: from 2019
Semester: summer
Points: summer s.:3
E-Credits: summer s.:3
Examination process: summer s.:
Hours per week, examination: summer s.:0/5, MC [HT]
Capacity: unknown / 30 (unknown)
Min. number of students: unlimited
State of the course: taught
Language: Czech
Teaching methods: full-time
Teaching methods: full-time
Level:  
Guarantor: Džuman Zbyněk Ing. Ph.D.
Stupák Michal Ing. Ph.D.
Class: Základní laboratoře
Interchangeability : N323055
Annotation -
Subject Chromatography and mass spectrometry: Laboratory is designed for students who have completed course Interpretation of chromatographic and mass-spectrometric data. The aim of the course is to practically introduce to students modern techniques for detection of compounds utilizing various instruments, data handling and interpretation, including statistical data processing (multivariate analysis). Laboratories are designed as single handle activities of students on their own projets.
Last update: Džuman Zbyněk (25.01.2018)
Aim of the course -

Students will be able to:

Prepare and plan experimental work in the modern laboratory, under the leadership perform the instrumental analysis, process the interpret the acquired data.

Last update: Džuman Zbyněk (25.01.2018)
Literature -

R: Picó Y.: Food Toxicants Analysis, Elsevier, 2007, ISBN: 978-0-444-52843-8.

R: Otleş S.: Handbook of Food Analysis Instruments, CRC, 2008, ISBN: 9781420045666.

R: de Hoffmann E., Stroobant V.: Mass Spectrometry - Principles and Applications, Wiley, 2002 ISBN: 9780471485667.

Last update: Džuman Zbyněk (14.09.2023)
Learning resources -

https://web.vscht.cz/poustkaj/

http://www.chem.arizona.edu/massspec/

http://www.ionsource.com/tutorial/spectut/spec1.htm

http://www.chemguide.co.uk/analysis/masspecmenu.html

http://webbook.nist.gov/chemistry/

http://www.chemspider.com/

http://www.massbank.jp/

http://metlin.scripps.edu/

Last update: Džuman Zbyněk (25.01.2018)
Requirements to the exam -

Within the extent of the syllabus.

Last update: Vlčková Martina (30.01.2018)
Syllabus -

1. Introduction, organization of laboratories, laboratory safety.

2-4. Project preparation (general introduction, practical introduction in the laboratory).

5. Task entry, individual preparation (literature search, procedures proposals).

6-12. Laboratory work - work on the project.

13. Project results processing.

14. Presentation of results, project defense.

Last update: Džuman Zbyněk (25.01.2018)
Registration requirements -

Interpretation of chromatographic and mass spectrometric data

Last update: Džuman Zbyněk (25.01.2018)
Course completion requirements -

Active participation in laboratories and final defense of the project including oral presentation.

Last update: Džuman Zbyněk (25.01.2018)
Teaching methods
Activity Credits Hours
Konzultace s vyučujícími 0.5 14
Účast v laboratořích (na exkurzi nebo praxi) 1 28
Obhajoba individuálního projektu 0.5 14
Práce na individuálním projektu 1 28
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