Subjects

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Chromatography and mass spectrometry: Laboratory - N323055

Title:	Laboratoř chromatografie a hmotnostní spektrometrie
Podoba výuky:	laboratory practicals
Guaranteed by:	Department of Food Analysis and Nutrition (323)
Faculty:	Faculty of Food and Biochemical Technology
Actual:	from 2023
Kolik má semestrů:	1
Semester:	summer
Points:	summer s.:3
E-Credits:	summer s.:3
Examination process:	summer s.:
Hours per week, examination:	summer s.:0/5, MC [HT]
Capacity:	unknown / unknown (unknown)
Maximální kapacita předmětu:	unlimited
Min. number of students:	unlimited
State of the course:	cancelled
Language:	Czech
Teaching methods:	full-time
Level:
Belongs to the student work of type:	projekt
Enroll for the course repeatedly:	- / - / - / 9

Guarantor:	Stránská Milena prof. Ing. Ph.D. Pulkrabová Jana prof. Ing. Ph.D.
Class:	Specializační laboratoř
Is interchangeable with:	M323022

Examination dates Schedule

Annotation -

Subject Chromatography and mass spectrometry: Laboratory is designed for students who have completed course Interpretation of chromatographic and mass-spectrometric data. The aim of the course is to practically introduce to students modern techniques for detection of compounds, data handling and interpretation, including statistical data processing (multivariate analysis). Laboratories are designed as single handle activities of students on their own projets.

Last update: Pulkrabová Jana (03.07.2013)

Literature -

R: Picó Y.: Food Toxicants Analysis, Elsevier, 2007, ISBN: 978-0-444-52843-8.

R: Otleş S.: Handbook of Food Analysis Instruments, CRC, 2008, ISBN: 9781420045666.

R: de Hoffmann E., Stroobant V.: Mass Spectrometry - Principles and Applications, Wiley, 2002 ISBN: 9780471485667.

R: Kaliszan R.: Structure and Retention in Chromatography: A Chemometric Approach (Chromatography: Principles & Practice Series), CRC, 1997 ISBN: 9789057020285.

Last update: Pulkrabová Jana (03.07.2013)

Syllabus -

1. Introduction, organization of laboratories, laboratory safety, project assignment

2. - 3. Preparation of project (selection methods, literature search

4. - 11. Laboratory work - work on the project

12. - 14. Data processing, preparation of the final project report

Last update: TAJ323 (28.08.2013)

Learning resources -

http://web.vscht.cz/cajkat/ICSD.html

http://www.chem.arizona.edu/massspec/

http://www.ionsource.com/tutorial/spectut/spec1.htm

http://www.chemguide.co.uk/analysis/masspecmenu.html

http://webbook.nist.gov/chemistry/

http://www.chemspider.com/

http://www.massbank.jp/

http://metlin.scripps.edu/

Last update: Pulkrabová Jana (03.07.2013)

Learning outcomes -

Students will be able to:

prepare and plan experimental work in the modern laboratory.

under the leadership to analyse organic compounds using the modern instruments.

process and interpret the measured data.

Last update: TAJ323 (16.08.2013)

Registration requirements -

Interpretation of chromatographic and spectrometric data

Last update: Pulkrabová Jana (03.07.2013)

Teaching methods
	Activity	Credits	Hours
	Účast v laboratořích (na exkurzi nebo praxi)	2	56
	Příprava na přednášky, semináře, laboratoře, exkurzi nebo praxi	0.5	14
	Práce na individuálním projektu	0.5	14
		3 / 3	84 / 84

Coursework assessment
Form	Significance
Regular attendance	50
Defense of an individual project	50