Structural Crystallography - N108011
Title: Strukturní krystalografie
Guaranteed by: Department of Solid State Chemistry (108)
Faculty: Faculty of Chemical Technology
Actual: from 2019
Semester: winter
Points: winter s.:3
E-Credits: winter s.:3
Examination process: winter s.:
Hours per week, examination: winter s.:2/0, Ex [HT]
Capacity: unknown / unknown (unknown)
Min. number of students: unlimited
State of the course: cancelled
Language: Czech
Teaching methods: full-time
Teaching methods: full-time
Note: course can be enrolled in outside the study plan
enabled for web enrollment
Guarantor: Hušák Michal doc. Dr. Ing.
Is interchangeable with: M108004
Examination dates   Schedule   
Annotation -
The aim of the course is to teach students how to obtain information about the complete structure of investigated compound using diffraction methods. The course is suitable for pharmacists, organic chemists but also inorganic chemists who need to analyse crystalline products.
Last update: Hušák Michal (02.09.2013)
Aim of the course -

Students will be able to:

Utilize the methodology of X-ray diffraction analysis in the form of their own experiments.

Interpret the results of X-ray diffraction analysis from databases and literature.

Propose appropriate analytical methods for the solution associated with the solid state phase's analysis.

Last update: Hušák Michal (02.09.2013)
Literature -

R:Kratochvíl B., Chemie a fyzika pevných látek I, VŠCHT Praha, 1994, 8070801964

R:Kratochvíl B., Jenšovský L., Úvod do krystalochemie, SNTL Praha, 1987, 0460887

Last update: TAJ108 (29.08.2013)
Learning resources -

R:Lectures in power-point form (actual version available by the lecturer)

Last update: TAJ108 (06.09.2013)
Teaching methods - Czech

28 hodin přednášek

Last update: Hušák Michal (06.11.2012)
Requirements to the exam - Czech

Účast na přednáškách.

Last update: Hušák Michal (25.02.2009)
Syllabus -

1. Crystal structure. Space groups, application, matrix representation.

2. Types of radiation used for crystallographic studies and their characteristics.

3. Sources of radiation for crystallographic studies.

4. Bragg equation, Evald construction.

5. Different arrangement of diffraction experiments, in terms of radiation used and sample type.

6. Atomic scattering factor, structure factor.

7. Measuring on the four-circle diffractometer.

8. Correction's of diffraction data.

9. Methods for solving the phase problem.

10. Structure refinement from the diffraction data.

11. Specific problems of biological macromolecules structures solution.

12. Solution of crystal structures from powder diffraction data. Rietveld method.

13. Methods for solving crystal structures based on electron microscopy.

14. Databases of crystallographic data.

Last update: Hušák Michal (02.09.2013)
Registration requirements -

Chemistry and Physics of Solids

Mathematics I

Last update: TAJ108 (06.09.2013)
Teaching methods
Activity Credits Hours
Konzultace s vyučujícími 0.5 14
Účast na přednáškách 1 28
Příprava na přednášky, semináře, laboratoře, exkurzi nebo praxi 0.5 14
Příprava na zkoušku a její absolvování 1 28
3 / 3 84 / 84
Coursework assessment
Form Significance
Oral examination 100