Subjects

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Organic Chemistry: Laboratory I - N110002

Title:	Laboratoř organické chemie I
Guaranteed by:	Department of Organic Chemistry (110)
Faculty:	Faculty of Chemical Technology
Actual:	from 2022
Semester:	both
Points:	3
E-Credits:	3
Examination process:
Hours per week, examination:	0/4, MC [HT]
Capacity:	winter:unknown / unknown (unknown) summer:unknown / unknown (unknown)
Min. number of students:	unlimited
State of the course:	cancelled
Language:	Czech
Teaching methods:	full-time
Teaching methods:	full-time
Level:
Is provided by:	B110005
Additional information:	http://Do termínů laboratoří se musí studenti přihlásit prostřednictvím SIS jako na termín zkoušky z Laboratoří OCH I
Note:	deregister from the exam date if a requisite was not fulfilled you can enroll for the course in winter and in summer semester

Guarantor:	Kozmík Václav Ing. CSc.
Class:	Základní laboratoře
Pre-requisite :	{x}, {x}
Interchangeability :	N110002A, N110502, Z110002
Is interchangeable with:	B110005, AB110005, N110002A
In complex pre-requisite:	AB110006, B110006

Examination dates Schedule

Annotation -

Students will learn about laboratory safety, basic laboratory equipment and experimental procedures used in organic chemistry. Working on several simple organic syntheses, students will acquire the requisite skills for the preparation and characterization of organic compounds. Final grade is based not only on the performance in the laboratory, but also on the knowledge of simple calculations (stoichiometry and preparation of solutions) and the chemical principles of procedures carried out.

Last update: MARTINUT (02.08.2013)

Aim of the course -

Students will be able to:

work safely in organic laboratory

carry out basic laboratory operations

combine the theoretical knowledge with experimental results

understand the system of organic synthesis - reaction planning, building a reaction apparatus, carrying out a reaction, isolation and characterization of products

write laboratory protocols

Last update: Cibulka Radek (19.08.2013)

Literature -

R: J. W. Zubrick, The Organic Chem Lab Survival Manual: A Student's Guide to Techniques, 5th Ed., Wiley 2001.0471387320

Last update: Cibulka Radek (05.02.2015)

Syllabus -

1. Laboratory safety and first aid instructions.

2. Laboratory rules, recordkeeping, protocols, essential calculations.

3. Basic laboratory equipment.

4. Building of reaction apparatuses.

5. Crystallization and filtration.

6. Organic solvents, extraction, drying, evaporation.

7. Stirring and heating under reflux.

8. One-step syntheses of various organic substances, isolation and identification of products.

9. Multi-step syntheses.

10. Operations under anhydrous conditions.

11. Distillation under ambient pressure.

12. Distillation under reduced pressure.

13. Melting point determination.

14. Gas chromatography.

Last update: MARTINUT (02.08.2013)

Learning resources -

Laboratory instructions

Last update: MARTINUT (02.08.2013)

Entry requirements -

Organic chemistry I or Organic Chemistry A and Inorganic Chemistry: Laboratory I.

Last update: Cibulka Radek (14.09.2016)

Registration requirements -

Organic chemistry I or Organic Chemistry A and Inorganic Chemistry: Laboratory I.

Last update: Cibulka Radek (14.09.2016)

Teaching methods
	Activity	Credits	Hours
	Účast v laboratořích (na exkurzi nebo praxi)	2	56
	Příprava na přednášky, semináře, laboratoře, exkurzi nebo praxi	1	28
		3 / 3	84 / 84

Coursework assessment
Form	Significance
Regular attendance	40
Report from individual projects	30
Continuous assessment of study performance and course -credit tests	30