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Last update: Kvíčala Jaroslav prof. Ing. CSc. (22.08.2013)
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Last update: Cibulka Radek prof. Ing. Ph.D. (22.08.2013)
Students will be able to: use advanced glass-blowing techniques perform the experiments at low temperature under inert conditions using inert lines and septum techniques perform the experiments in sealed ampules perform the experiments with low-boiling liquids under inert conditions |
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Last update: Cibulka Radek prof. Ing. Ph.D. (28.08.2013)
R: Jaroslav Kvíčala: Laboratorní technika organické chemie, VŠCHT Praha, Praha 2007. ISBN10: 8070803223, ISBN13: 9788070803223. |
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Last update: Kvíčala Jaroslav prof. Ing. CSc. (22.08.2013)
Printed experiment details |
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Last update: Cibulka Radek prof. Ing. Ph.D. (24.08.2012)
V rámci tohoto předmětu posluchači absolvují týdenní kurz laboratorní techniky (organizováno turnusově Po-Pá 8:00 � 17:00, celkem 45 hodin). Další náplní kurzu je práce ve specializovaných laboratořích a literární rešerše (8 hodin týdně � 12 týdnů). Organizaci specializovaných laboratoří si studenti dohodnou s vedoucím práce. |
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Last update: Kvíčala Jaroslav prof. Ing. CSc. (22.08.2013)
1. Advanced glass-blowing techniques, making Schlenk flask. 2. Protecting of propargyl alcohol with dihydropyran, control of purity of the product by NMR spectroscopy. 3. Alkylation of protected propargyl alcohol with unknown alkyl iodide,identification of the product by NMR spectroscopy. 4. Deprotection of protected alkynyl alcohol, control of purity of the product by NMR spectroscopy. 5. Determination of unknown concentration of butyllithium. 6. Work under low temperature, synthesis of unknown kinetic silyl enol ether, isolation of the product by microdistillation, identification of the product by NMR spectroscooy. 7. Work in sealed ampules, synthesis of unknown thermodynamic silyl enol ether, isolation of the product by microdistillation, identification of the product by NMR spectroscooy. 8. Katalytic hydrogenation of alkynol to cis-alkenol. 9. Work with low-boiling liquds, reduction of alkynol with sodium in liquid ammonia. 10. Work on the research project in the tutor laboratory. |
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Last update: Kvíčala Jaroslav prof. Ing. CSc. (22.08.2013)
Organic Chemistry II, Laboratory of Organic Chemistry I |
Teaching methods | ||||
Activity | Credits | Hours | ||
Účast v laboratořích (na exkurzi nebo praxi) | 5 | 140 | ||
Obhajoba individuálního projektu | 0.1 | 2 | ||
Práce na individuálním projektu | 1.9 | 54 | ||
7 / 7 | 196 / 196 |
Coursework assessment | |
Form | Significance |
Regular attendance | 20 |
Report from individual projects | 20 |
Defense of an individual project | 60 |