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The aim of this course is to familiarize students in practice with various analytical techniques, which were theoretically lectured in previous courses. The students will learn about the modern instrumental technique and its use in analytical practice in individual exercises.
Last update: Schulzová Věra (08.07.2013)
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Students will be able to:
Last update: TAJ323 (16.08.2013)
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Completed all laboratory tasks (with the exception of a maximum of two absences excused by a doctor), all protocols elaborated and submitted Last update: Schulzová Věra (02.07.2013)
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R: Study materials for courses: Analytical Chemistry I - D. Kealey, P. J. Haines: Analytical Chemistry, BIOS Sci. Publ., Oxford 2002, ISBN 1-85996-189-4 Food and Natural Products Analysis - http://web.vscht.cz/hajslovj/AP_sylabus.html A: http://www.scribd.com/doc/30735048/Food-Analysis-by-HPLC-2ed-Nollet A: Meyer V., Practical High-Performance Liquid Chromatography, Wiley 2010, ISBN-10: 0470682175 A: Weston A., Brown P.R, HPLC and CE: Principles and Practice, Amazon 1997, ISBN-10: 0121366405 A: Pavia D.L., Lapman G.M., Kriz G.S., Vyvyan J.R., Introduction to Spectroscopy, Brooks/Cole, Belmont 2009,ISBN-13: 978-0-495-11478-9 A: Aras N.K., Ataman O.Y., Trace Element Analysis of Food and Diet, RSC, Cambridge, 2006,ISBN 0-85404-576-7 A: Nielsen S.S. (ed.)Food Analysis 4th edition, Springer, 2010, ISBN 978-1-4419-1478-1, e-zdroj VŠCHT A: Otles S. (ed.), Handbook of Food Analysis Instruments. CRC Press, Boca Raton, USA, 2009, ISBN 9781420045673, e-zdroje VŠCHT A: Wrolstad R.E. et al., Handbook of Food Analytical Chemistry, Wiley, 2005, ISBN 9780471663782, e-zdroj VŠCHT Last update: Schulzová Věra (03.07.2013)
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1. Introduction, organizational issues, work safety. 2. Gas chromatography. 3. Gas chromatography (GC/FID). 4. Gas chromatography (GC/MS). 5. Ion selective electrodes. 6. High performance liquid chromatography. 7. High performance liquid chromatography I (HPLC/UV). 8. High performance liquid chromatography II (special detectors). 9. Spectrophotometry I. 10. Spectrophotometry II. 11. Atomic absorption spectrophotometry. 12. Infrared spectrophotometry. 13. Image analysis. 14. Electromigration methods. Last update: TAJ323 (16.08.2013)
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http://sbirka.vscht.cz/ http://eur-lex.europa.eu/cs/index.htm http://www.sciencedirect.com/science/book/9780121366407 Commercial firm literature http://web.vscht.cz/schulzov/ Last update: Schulzová Věra (03.07.2013)
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Analytical Chemistry, Food and Natural Products Analysis: Laboratory Last update: Schulzová Věra (02.07.2013)
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Teaching methods | ||||
Activity | Credits | Hours | ||
Účast v laboratořích (na exkurzi nebo praxi) | 3 | 84 | ||
Příprava na přednášky, semináře, laboratoře, exkurzi nebo praxi | 1 | 28 | ||
4 / 4 | 112 / 112 |
Coursework assessment | |
Form | Significance |
Regular attendance | 50 |
Report from individual projects | 50 |