SubjectsSubjects(version: 853)
Course, academic year 2019/2020
  
Methods of Structural and Surface Analysis - AM402004
Title: Methods of Structural and Surface Analysis
Guaranteed by: Department of Analytical Chemistry (402)
Actual: from 2019
Semester: winter
Points: winter s.:3
E-Credits: winter s.:3
Examination process: winter s.:
Hours per week, examination: winter s.:2/0 Ex [hours/week]
Capacity: unknown / unknown (unknown)
Min. number of students: unlimited
Language: English
Teaching methods: full-time
Level:  
For type: Master's (post-Bachelor)
Additional information: http://www.vscht.cz/anl/matejka/
Note: course can be enrolled in outside the study plan
enabled for web enrollment
Guarantor: Matějka Pavel prof. Dr. RNDr.
Interchangeability : M402004, N402014
Is interchangeable with: M402004
Annotation -
Last update: Kubová Petra Ing. (22.01.2018)
This subject comprises the basic terms, related to the molecular structure analysis and surface analysis. It brings a survey of individual techniques and offered information. Techniques of the surface analysis and imaging, including the scanning probe (near-field) microanalysis, are the second key part of this survey. In some cases it is an extension of knowledge gained in the basic courses of Analytical chemistry I and II.
Aim of the course -
Last update: Kubová Petra Ing. (22.01.2018)

Students will be able to:

Describe and explain the principles and instrumentation of following techniques: photoelectron spectroscopy, Auger spectroscopy, X-ray fluorescence analysis, electron microscopy, scanning probe microscopy, X-ray, electron and neutron diffraction, secondary ion mass spectrometry, infrared and Raman microspectrometry and NMR spectrometry/relaxometry focusing on solids.

Know examples of practical applications of individual techniques of structural and surface analysis.

Literature -
Last update: Matějka Pavel prof. Dr. RNDr. (21.02.2018)

R:Modern Instrumental Analysis, ed. S. Ahuja, N. Jespersen, Comprehensive Analytical Chemistry Vol. 47 (2006), p. 1-864, ISBN: 978-0-444-52259-7, https://www.sciencedirect.com/science/handbooks/0166526X/47 (available online at VSCHT)

A:Non-Destructive Microanalysis of Cultural Heritage materials, ed. S. Ahuja, N. Jespersen, Comprehensive Analytical Chemistry Vol. 42 (2004), p. 1-800, ISBN: 978-0-444-50738-9, https://www.sciencedirect.com/science/handbooks/0166526X/42 (available online at VSCHT)

A:R.L. McCreery: Raman Spectroscopy for Chemical Analysis, Wiley 2000, Online ISBN: 9780471721642, http://onlinelibrary.wiley.com/book/10.1002/0471721646 (available online at VSCHT)

A:L. A. Casper, C. J. Powell: Industrial Applications of Surface Analysis, vol. 199, ACS 1982, eISBN: 9780841209411, https://pubs.acs.org/doi/book/10.1021/bk-1982-0199 (available online at VSCHT)

A:Sam Zhang, Lin Li, Ashok Kumar: Materials Characterization Techniques, CRC Press Boca Raton 2009, ISBN 978-1-4200-4294-8

Learning resources -
Last update: Kubová Petra Ing. (22.01.2018)

electronic materials - slides for lectures - http://www.vscht.cz/anl/matejka/#povrch

Syllabus -
Last update: Matějka Pavel prof. Dr. RNDr. (21.02.2018)

1. Fundamental terms of structural and surface analysis

2. Surface analysis methods based on electron detection (XPS, UPS)

3. Surface analysis methods based on electron detection (Auger spectroscopy)

4. Methods of electron microscopy and chemical analysis (EDX, WDX)

5. Methods of scanning probe microscopy (AFM, STM, SNOM)

6. Surface analysis methods based on ion detection (SIMS)

7. Methods of X-ray diffraction

8. Electron and neutron diffraction

9. Techniques of infrared and Raman spectrometry

10. Infrared and Raman microspectrometry, mapping and imaging

11. Surface-enhanced vibrational spectroscopies

12. NMR spectroscopy and molecular structure

13. Solid-state NMR spectroscopy

14. NMR analysis in inhomogeneous fields, mobile NMR

Registration requirements -
Last update: Kubová Petra Ing. (22.01.2018)

none

Course completion requirements -
Last update: Matějka Pavel prof. Dr. RNDr. (21.02.2018)

It is compulsory to pass a written test and final oral examination.

Teaching methods
Activity Credits Hours
Konzultace s vyučujícími 0,5 14
Účast na přednáškách 1 28
Příprava na přednášky, semináře, laboratoře, exkurzi nebo praxi 0,5 14
Příprava na zkoušku a její absolvování 1 28
3 / 3 84 / 84
Coursework assessment
Form Significance
Regular attendance 10
Examination test 40
Oral examination 50

 
VŠCHT Praha