SubjectsSubjects(version: 853)
Course, academic year 2019/2020
  
Methods of Structural and Surface Analysis - M402004
Title: Metody strukturní a povrchové analýzy
Guaranteed by: Department of Analytical Chemistry (402)
Actual: from 2019
Semester: winter
Points: winter s.:3
E-Credits: winter s.:3
Examination process: winter s.:
Hours per week, examination: winter s.:2/0 Ex [hours/week]
Capacity: unlimited / unknown (unknown)
Min. number of students: unlimited
Language: Czech
Teaching methods: full-time
Level:  
For type: Master's (post-Bachelor)
Additional information: http://www.vscht.cz/anl/matejka/
Note: course can be enrolled in outside the study plan
enabled for web enrollment
Guarantor: Matějka Pavel prof. Dr. RNDr.
Interchangeability : AM402004, N402014
Is interchangeable with: AM402004
Annotation -
Last update: Pátková Vlasta (05.01.2018)
This subject comprises the basic terms, related to the molecular structure analysis and surface analysis. It brings a survey of individual techniques and offered information. Techniques of the surface analysis and imaging, including the scanning probe (near-field) microanalysis, are the second key part of this survey. In some cases it is an extension of knowledge gained in the basic courses of Analytical chemistry I and II.
Aim of the course -
Last update: Pátková Vlasta (05.01.2018)

Students will be able to:

Describe and explain the principles and instrumentation of following techniques: photoelectron spectroscopy, Auger spectroscopy, X-ray fluorescence analysis, electron microscopy, scanning probe microscopy, X-ray, electron and neutron diffraction, secondary ion mass spectrometry, infrared and Raman microspectrometry and NMR spectrometry/relaxometry focusing on solids.

Know examples of practical applications of individual techniques of structural and surface analysis.

Literature -
Last update: Pátková Vlasta (05.01.2018)

R: R.L. McCreery: Raman Spectroscopy for Chemical Analysis, Wiley 2000 (available online at VSCHT)

Modern Instrumental Analysis, ed. S. Ahuja, N. Jespersen, Comprehensive Analytical Chemistry Vol. 47 (2006), p. 1-864 (available online at VSCHT)

A: Non-Destrictive Microanalysis of Cultural Heritage materials, ed. S. Ahuja, N. Jespersen, Comprehensive Analytical Chemistry Vol. 42 (2004), p. 1-800 (available online at VSCHT)

A: L. A. Casper, C. J. Powell: Industrial Applications of Surface Analysis, vol. 199, ACS 1982 (available online at VSCHT)

Learning resources -
Last update: Pátková Vlasta (05.01.2018)

electronic materials - slides for lectures - http://www.vscht.cz/anl/matejka/#povrch

Teaching methods - Czech
Last update: Matějka Pavel prof. Dr. RNDr. (14.02.2018)

Přednášky

Syllabus -
Last update: Pátková Vlasta (05.01.2018)

1. Fundamental terms

2. Structure and geometry of molecules

3. Symmetry, point groups

4. Linear and circular polarized electromagnetic radiation, chirooptical methods

5. Infrared and Raman spectroscopy

6. Microwave spectroscopy

7. NMR spectrometry

8. Mass spectrometry

9. Crystal structure

10. X-ray and electron diffraction

11. Surface analysis methods based on electron detection

12. Surface analysis methods based on ion detection

13. Surface analysis methods based on photon detection

14. Scanning microscopy methods

Registration requirements -
Last update: Pátková Vlasta (05.01.2018)

none

Course completion requirements - Czech
Last update: Matějka Pavel prof. Dr. RNDr. (21.02.2018)

Složení zkoušky (písemný test, ústní pohovor)

Teaching methods
Activity Credits Hours
Konzultace s vyučujícími 0,5 14
Účast na přednáškách 1 28
Příprava na přednášky, semináře, laboratoře, exkurzi nebo praxi 0,5 14
Příprava na zkoušku a její absolvování 1 28
3 / 3 84 / 84
Coursework assessment
Form Significance
Regular attendance 10
Examination test 30
Oral examination 60

 
VŠCHT Praha