SubjectsSubjects(version: 875)
Course, academic year 2019/2020
  
Inorganic Chemistry: Laboratory I - B101004
Title: Laboratoř anorganické chemie I
Guaranteed by: Department of Inorganic Chemistry (101)
Actual: from 2019
Semester: summer
Points: summer s.:3
E-Credits: summer s.:3
Examination process: summer s.:
Hours per week, examination: summer s.:0/4 MC [hours/week]
Capacity: unknown / unlimited (unknown)
Min. number of students: unlimited
Language: Czech
Teaching methods: full-time
Level:  
For type: Bachelor's
Old code: ACH1L
Note: deregister from the exam date if a requisite was not fulfilled
enabled for web enrollment
Guarantor: Mastný Libor Ing. CSc.
Jakeš Vít Ing. Ph.D.
Pre-requisite : {prerekvizita pro Laboratoř z anorganické chemie I}, {x}
Interchangeability : AB101004, N101003, N101003A
Z//Is interchangeable with: B101004Z
XP//In complex pre-requisite: B110005, N110002, N110002A
This subject contains the following additional online materials
Annotation -
Last update: Jakeš Vít Ing. Ph.D. (29.01.2018)
Students are acquainted with the principles of work safety, basic laboratory equipment and basic experimental procedures. Preparation tasks and qualitative chemical reactions complement students' theoretical knowledge of the characteristic properties of the elements and compounds.
Aim of the course -
Last update: Jakeš Vít Ing. Ph.D. (29.01.2018)

Students will be able

  • to move safely in a laboratory;
  • to perform basic laboratory procedures;
  • to combine theoretical knowledge with experimental outputs;
  • to evaluate independently results of their work and make a detailed task description in the final record.
Literature -
Last update: Jakeš Vít Ing. Ph.D. (01.08.2019)

V. Jakeš a kol.: Laboratoř anorganické chemie I, VŠCHT Praha, 2018, ISBN: 978-80-7592-015-7 (available for download at: https://e-learning.vscht.cz/pluginfile.php/39052/mod_resource/content/3/LACH_I_skriptum_Jakeskol_2ed%282019%29.pdf)

D. Sýkorová, L. Mastný: Návody pro laboratoře z anorganické chemie, VŠCHT Praha, 2001, reprint 2009, ISBN: 80-7080-452-1

V. Flemr, E. Holečková: Úlohy z názvosloví a chemických výpočtů v anorganické chemii, VŠCHT Praha, 2001, ISBN: 80-7080-435-1

Learning resources -
Last update: Jakeš Vít Ing. Ph.D. (29.01.2018)

Programme of the Inorganic Chemistry: Laboratory I course and preparatory processes (video): https://e-learning.vscht.cz/course/view.php?id=40

Laboratory records: https://e-learning.vscht.cz/mod/url/view.php?id=3906

CLP pictograms for compounds and mixtures: https://prezi.com/embed/9pbb6hy3_was/?bgcolor=ffffff&lock_to_path=1&autoplay=no&autohide_ctrls=0

Safety in laboratory - video: https://e-learning.vscht.cz/mod/folder/view.php?id=3002

Basic laboratory procedures - video: https://e-learning.vscht.cz/mod/folder/view.php?id=3001

Requirements to the exam -
Last update: Jakeš Vít Ing. Ph.D. (13.02.2018)
  • regular tests in the beginning of each laboratory day (theoretical background and laboratory calculation)
  • final test (knowledge based on laboratory work and laboratory calculation)
  • reports from chosen laboratory tasks

Syllabus -
Last update: Jakeš Vít Ing. Ph.D. (29.01.2018)

1. Work safety in laboratory, laboratory rules, laboratory records.

2. Basic laboratory equipment.

3. Essential laboratory procedures - dissolution, filtration, evaporation, precipitation, decantation, work with a test tube.

4. Essential laboratory operations - crystallization, weighing, determination of density, pH determination.

5. Oxidation-reduction reactions - carried out in solution and in solid state.

6. Chemistry of non-metals - reactions of non-metals and their compounds.

7. Preparation of important compounds of selected elements and their reactions.

8. Important qualitative reactions of anions and their determination in unknown samples.

9. Chemistry of metals - reactions of metals and their compounds.

10. Coordination compounds of transition metals.

11. Qualitative reactions of cations, their separation and identification in unknown samples.

12. Mass balance of preparative experiments.

Registration requirements
Last update: Jakeš Vít Ing. Ph.D. (01.08.2019)

General and Inorganic Chemistry I (AB101001)

Chemical and Balance Calculation (AB101003)

Course completion requirements -
Last update: Mastný Libor Ing. CSc. (21.02.2018)

The subject is finished by completion of all laboratory works and continuous tests, submission of protocols and fulfillment of the finish test.

  • regular tests in the beginning of each laboratory day (theoretical background and laboratory calculation)
Teaching methods
Activity Credits Hours
Účast v laboratořích (na exkurzi nebo praxi) 2 56
Příprava na přednášky, semináře, laboratoře, exkurzi nebo praxi 1 28
3 / 3 84 / 84
Coursework assessment
Form Significance
Regular attendance 30
Report from individual projects 10
Examination test 30
Continuous assessment of study performance and course -credit tests 30

 
VŠCHT Praha