SubjectsSubjects(version: 853)
Course, academic year 2019/2020
  
Elemental analysis - N402070
Title: Prvková analýza
Guaranteed by: Department of Analytical Chemistry (402)
Actual: from 2013
Semester: winter
Points: winter s.:3
E-Credits: winter s.:3
Examination process: winter s.:
Hours per week, examination: winter s.:2/0 Ex [hours/week]
Capacity: unlimited / unknown (unknown)
Min. number of students: unlimited
Language: Czech
Teaching methods: full-time
Level:  
For type:  
Guarantor: Mestek Oto prof. Ing. CSc.
Šiškanova Taťjana doc. Mgr. CSc.
Is interchangeable with: M402024
This subject contains the following additional online materials
Annotation -
Last update: Mestek Oto prof. Ing. CSc. (15.09.2013)
Course is focused on basic methods of analysis of elements: chemical analysis (titration, gravimetric, photometric method), spectroscopic methods (atomic absorption, fluorescence, emission and mass spectrometry) and electrochemical methods (potentiometry, voltammetry). Attention is also paid to the preparation of samples for analysis.
Aim of the course -
Last update: VED402 (16.12.2013)

Students gain theoretical knowledge of various methods of elemental analysis: gravimetric and titration methods, optical spectroscopy (absorption, fluorescence and emission spectroscopy), mass spectrometry and electroanalytical methods. Become familiar with the techniques of preparation of samples for analysis and the issue of ensuring clean environment in the trace lab. In addition to determining the total element concentrations, they are also familiar with the methods of speciation analysis using a combination of spectral and separation methods.

Literature -
Last update: VED402 (01.10.2013)

R: Cullen M.: Atomic Spectroscopy in Elemental Analysis

R: Skoog D.A., West D.M., Holler F.J.: Analytical chemistry

Learning resources -
Last update: Mestek Oto prof. Ing. CSc. (03.09.2013)

http://web.vscht.cz/~koplikr/Atomov%c3%a1%20%20spektrometrie.pdf

Requirements to the exam -
Last update: Mestek Oto prof. Ing. CSc. (15.09.2013)

Students complete oral exam.

Syllabus -
Last update: Mestek Oto prof. Ing. CSc. (18.05.2012)

1 Gravimetry

2 Titrimetry: acidimetry anad alkalimetry, chelatometry, argentometry

3 Titrimetry: oxidimetry

4 Photometry

5 Atomic absorption spektroscopy with flame atomisation

6 Atomic absorption spektroscopy with electrotermic atomisation

7 Atomic fluorescence spektroscopy and flame emission spectroscopy

8 Inductively coupled plasma optical emission spectroscopy

9 Inductively coupled plasma mass spectroscopy

10 Speciation analysis of trace elements

11 Potentiometry, pH determination, ion selective electrodes

12 Coulometry

13 Voltametry, polarography

14 Sample preparation and experiments in elemental analysis

Registration requirements -
Last update: VED402 (16.12.2013)

Basic knowledge of analytical chemistry

Teaching methods
Activity Credits Hours
Konzultace s vyučujícími 0,2 6
Účast na přednáškách 1 28
Příprava na přednášky, semináře, laboratoře, exkurzi nebo praxi 0,5 14
Příprava na zkoušku a její absolvování 1,3 36
3 / 3 84 / 84
Coursework assessment
Form Significance
Oral examination 100

 
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